Title:
METHOD FOR PRODUCING PURIFIED LACTIC ACID SOLUTION
Document Type and Number:
WIPO Patent Application WO/2012/081112
Kind Code:
A1
Abstract:
The invention is capable of concentrating calcium lactate in a solution containing lactic acid obtained by fermentation in the form of calcium lactate at low cost and reduces the thermal degradation of impurities and the optical isomerization of lactic acid. A calcium lactate-containing solution containing lactic acid obtained by fermentation in the form of calcium lactate is subjected to concentration and purification by a method comprising (1) a step of concentrating calcium lactate by removing water contained in the calcium lactate-containing solution from the solution with a reverse osmotic membrane, (2) a step of separating calcium as calcium sulfate by adding sulfuric acid to the thus obtained concentrated liquid of calcium lactate after the step of concentration with a reverse osmotic membrane, and (3) a step of removing soluble impurities by ion exchange after the step of separation of calcium sulfate.
Inventors:
OKA KENICHIRO (JP)
MATSUO TOSHIAKI (JP)
KAMIKAWA MASAYUKI (JP)
OKAMOTO NARUYASU (JP)
KONDO TAKEYUKI (JP)
SUZUKI KAZUTAKA (JP)
MATSUO TOSHIAKI (JP)
KAMIKAWA MASAYUKI (JP)
OKAMOTO NARUYASU (JP)
KONDO TAKEYUKI (JP)
SUZUKI KAZUTAKA (JP)
Application Number:
PCT/JP2010/072694
Publication Date:
June 21, 2012
Filing Date:
December 16, 2010
Export Citation:
Assignee:
HITACHI PLANT TECHNOLOGIES LTD (JP)
OKA KENICHIRO (JP)
MATSUO TOSHIAKI (JP)
KAMIKAWA MASAYUKI (JP)
OKAMOTO NARUYASU (JP)
KONDO TAKEYUKI (JP)
SUZUKI KAZUTAKA (JP)
OKA KENICHIRO (JP)
MATSUO TOSHIAKI (JP)
KAMIKAWA MASAYUKI (JP)
OKAMOTO NARUYASU (JP)
KONDO TAKEYUKI (JP)
SUZUKI KAZUTAKA (JP)
International Classes:
C12P7/56; C07C51/42
Foreign References:
JP2003511360A | 2003-03-25 | |||
US5766439A | 1998-06-16 | |||
JP2001506274A | 2001-05-15 | |||
JP2007124931A | 2007-05-24 |
Other References:
LIEW M.K.H.: "Separation and purification of lactic acid: fundamental studies on the reverse osmosis down-stream process.", REPORTS OF THE HOKKAIDO NATIONAL INDUSTRIAL RESEARCH INSTITUTE, 1997, pages 32 - 40
Attorney, Agent or Firm:
HIRAKI YUSUKE (JP)
Yusuke Hiraki (JP)
Yusuke Hiraki (JP)
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Claims: