Title:
METHOD FOR SYNTHESIS OF TKX-50 USING INSENSITIVE INTERMEDIATE
Document Type and Number:
WIPO Patent Application WO/2020/040448
Kind Code:
A1
Abstract:
The present invention relates to a method for synthesis of TKX-50 using an insensitive intermediate and, more specifically, to a method for producing TKX-50, the method comprising the steps of: preparing DCG as a starting material; forming a THP-DAG intermediate from the DCG; and synthesizing TKX-50 through the THP-DAG intermediate.
Inventors:
KWON KUK TAE (KR)
LEE WOONG HEE (KR)
SHIM JEONG SUB (KR)
LEE SO JUNG (KR)
LEE WOONG HEE (KR)
SHIM JEONG SUB (KR)
LEE SO JUNG (KR)
Application Number:
PCT/KR2019/009723
Publication Date:
February 27, 2020
Filing Date:
August 05, 2019
Export Citation:
Assignee:
AGENCY DEFENSE DEV (KR)
International Classes:
C07D257/04; C06B25/34
Foreign References:
| CN104829548A | 2015-08-12 | |||
| CN103524444A | 2014-01-22 |
Other References:
SABATINI, J. J.: "Recent advances in the synthesis of high explosive materials", CRYSTALS, vol. 6, 2016, pages 1 - 22, XP055688220
FISCHER, N.: "Pushing the limits of energetic materials-the synthesis and characterization of dihydroxylammonium 5,5'-bistetrazole-1,1'-diolate", JOURNAL OF MATERIALS CHEMISTRY, vol. 22, 2012, XP055688234
LEE, W. H.: "Safe synthesis of TKX-50 using an insensitive intermediate", PROPELLANTS, EXPLOSIVES, PYROTECHNICS, vol. 44, no. 11, 2019, pages 1478 - 1481, XP055688264
FISCHER, N.: "Pushing the limits of energetic materials-the synthesis and characterization of dihydroxylammonium 5,5'-bistetrazole-1,1'-diolate", JOURNAL OF MATERIALS CHEMISTRY, vol. 22, 2012, XP055688234
LEE, W. H.: "Safe synthesis of TKX-50 using an insensitive intermediate", PROPELLANTS, EXPLOSIVES, PYROTECHNICS, vol. 44, no. 11, 2019, pages 1478 - 1481, XP055688264
Attorney, Agent or Firm:
MUHANN PATENT & LAW FIRM (KR)
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