Title:
METHOD FOR VAPOR PHASE CATALYTIC OXIDATION
Document Type and Number:
WIPO Patent Application WO/2003/057653
Kind Code:
A1
Abstract:
A method for vapor phase catalytic oxidation involving using a fixed bed multi-tube heat-exchanger type reactor having a plurality of reaction tubes, feeding a raw material gas for reaction to the inside of the reaction tube packed with a catalyst to produce a reaction product gas, characterized in that the pressure loss of each reaction tube having a catalyst packed therein is adjusted in a manner wherein a reaction tube showing a pressure loss less than an average pressure loss for the total reaction tubes is additionally packed with an inert material in its portion near the entrance of a raw material gas, or is removed of the catalyst and re-packed with the catalyst, and a reaction tube showing a pressure loss greater than the above average value is removed of the catalyst and then re-packed with the catalyst, so as for the each reaction tube to show a pressure loss within the range of ± 20 % of the average value. The method can provide a vapor phase catalytic oxidation method which is almost free of variations in the reaction states in respective reaction tubes.
Inventors:
YADA SHUHEI (JP)
GORIKI MASAYASU (JP)
HOSAKA HIROCHIKA (JP)
JINNO KIMIKATSU (JP)
SAITO TERUO (JP)
SUZUKI YOSHIRO (JP)
GORIKI MASAYASU (JP)
HOSAKA HIROCHIKA (JP)
JINNO KIMIKATSU (JP)
SAITO TERUO (JP)
SUZUKI YOSHIRO (JP)
Application Number:
PCT/JP2002/013372
Publication Date:
July 17, 2003
Filing Date:
December 20, 2002
Export Citation:
Assignee:
MITSUBISHI CHEM CORP (JP)
YADA SHUHEI (JP)
GORIKI MASAYASU (JP)
HOSAKA HIROCHIKA (JP)
JINNO KIMIKATSU (JP)
SAITO TERUO (JP)
SUZUKI YOSHIRO (JP)
YADA SHUHEI (JP)
GORIKI MASAYASU (JP)
HOSAKA HIROCHIKA (JP)
JINNO KIMIKATSU (JP)
SAITO TERUO (JP)
SUZUKI YOSHIRO (JP)
International Classes:
B01J8/00; B01J8/06; B01J23/28; B01J23/31; B01J23/887; B01J35/02; C07C45/33; C07C45/35; C07C27/14; C07C51/25; (IPC1-7): C07C27/14; C07C45/33; C07C45/35; C07C47/22; C07C51/25; C07C57/05; C07B33/00; B01J8/02
Foreign References:
JPS60136344U | 1985-09-10 | |||
JPH067669A | 1994-01-18 | |||
JPH0597730A | 1993-04-20 | |||
US4461327A | 1984-07-24 | |||
EP1156027A1 | 2001-11-21 | |||
JPH05261272A | 1993-10-12 | |||
JP2002306953A | 2002-10-22 | |||
JP2003001094A | 2003-01-07 |
Other References:
See also references of EP 1466883A4
Attorney, Agent or Firm:
Toyama, Tsutomu (4-10 Higashi Nihonbashi 3-chom, Chuo-ku Tokyo, JP)
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