Title:
NANOGOLD-LOADED TUNGSTEN OXIDE-SILVER SULFIDE COMPOSITE MATERIAL AND PREPARATION METHOD THEREFOR AND APPLICATION THEREOF
Document Type and Number:
WIPO Patent Application WO/2023/045082
Kind Code:
A1
Abstract:
The present invention relates to a nanogold-loaded tungsten oxide-silver sulfide composite material and a preparation method therefor and an application thereof. The method comprises: hydrothermally growing a WO3 nanometer square sheet on FTO glass by means of a solution method; then growing Ag2S on the surface of the WO3 nanometer square sheet by means of a chemical bath deposition method; and finally, depositing on Ag2S/WO3 by means of a constant potential, and performing constant potential deposition of Au nanoparticles to prepare the nanogold-loaded tungsten oxide-silver sulfide composite material. The composite material also has good absorbance in a visible light region, can avoid inactivation of biomolecules caused by ultraviolet light, and can be applied to photoelectrochemical detection of tumor markers CA15-3.
Inventors:
ZHANG MIN (CN)
LIU CHAOQIAO (CN)
CHENG FALIANG (CN)
XIE SHILEI (CN)
XIE DONG (CN)
LIU PENG (CN)
WANG SHOUSHAN (CN)
LIU CHAOQIAO (CN)
CHENG FALIANG (CN)
XIE SHILEI (CN)
XIE DONG (CN)
LIU PENG (CN)
WANG SHOUSHAN (CN)
Application Number:
PCT/CN2021/135092
Publication Date:
March 30, 2023
Filing Date:
December 02, 2021
Export Citation:
Assignee:
UNIV DONGGUAN TECHNOLOGY (CN)
International Classes:
G01N27/26; B82Y30/00; B82Y40/00; G01N27/30; G01N33/574
Foreign References:
| CN110779976A | 2020-02-11 | |||
| CN109926068A | 2019-06-25 |
Other References:
刘超巧 等 (LIU, CHAOQIAO ET AL.): "基于WO3@Ag2S@AuNPs核壳纳米复合物构建的新型光电化学免疫传感器用于肿瘤标记物CA15-3的检测 (Non-official translation: A Novel Photochemoimmunosensor Based on WO3@Ag2S@AuNPs Core-shell Nanocomplex for the Detection of Tumor Marker CA15-3)", 第十六届全国有机电化学与电化学工业学术会议论文集 (THESES OF 16TH NATIONAL SYMPOSIUM ON ORGANIC ELECTROCHEMISTRY AND ELECTROCHEMICAL INDUSTRY), 12 October 2018 (2018-10-12)
KE XI, YANG MENGMENG, WANG WEIZHE, LUO DONGXIANG, ZHANG MENGLONG: "Incidence Dependency of Photonic Crystal Substrate and Its Application on Solar Energy Conversion: Ag2S Sensitized WO3 in FTO Photonic Crystal Film", MATERIALS, vol. 12, no. 16, pages 2558, XP093051846, DOI: 10.3390/ma12162558
TORAD EMAN, ISMAIL EMAN H., MOHAMED MOHAMED MOKHTAR, KHALIL MOSTAFA M.H.: "Tuning the redox potential of Ag@Ag2O/WO3 and Ag@Ag2S/WO3 photocatalysts toward diclofenac oxidation and nitrophenol reduction", MATERIALS RESEARCH BULLETIN, ELSEVIER, KIDLINGTON., GB, vol. 137, 1 May 2021 (2021-05-01), GB , pages 111193, XP093051851, ISSN: 0025-5408, DOI: 10.1016/j.materresbull.2020.111193
KE XI, YANG MENGMENG, WANG WEIZHE, LUO DONGXIANG, ZHANG MENGLONG: "Incidence Dependency of Photonic Crystal Substrate and Its Application on Solar Energy Conversion: Ag2S Sensitized WO3 in FTO Photonic Crystal Film", MATERIALS, vol. 12, no. 16, pages 2558, XP093051846, DOI: 10.3390/ma12162558
TORAD EMAN, ISMAIL EMAN H., MOHAMED MOHAMED MOKHTAR, KHALIL MOSTAFA M.H.: "Tuning the redox potential of Ag@Ag2O/WO3 and Ag@Ag2S/WO3 photocatalysts toward diclofenac oxidation and nitrophenol reduction", MATERIALS RESEARCH BULLETIN, ELSEVIER, KIDLINGTON., GB, vol. 137, 1 May 2021 (2021-05-01), GB , pages 111193, XP093051851, ISSN: 0025-5408, DOI: 10.1016/j.materresbull.2020.111193
Attorney, Agent or Firm:
DONGGUAN HENGCHENG IP AGENCY CO., LTD (CN)
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