' The invention concerns a powder pipette for taking out samples of a pulverulent material. * During the manufacturing of pulverulent products

5 samples of the product are currently taken out to be analyzed to make sure that the intended quality of the product is maintained.

Such samples may be taken out manually by simply taking out a spoonful of the material and weighing out a 10 precise quantity for the analysis. Using a spoon of a size holding approximately the quantity wanted makes it possible to replace the precise weighing out by a simple weighing of the quantity taken out and set the result of the analysis in relation to the quantity used. 15 To make sure that material is not carried over from one sample to another it is preferred to use a new spoon for each sample. As the dust of the product may be harmful to the person taking out the samples, a mechanical sampler which in isolation can take out the samples and place them in test tubes 20 or other appropriate vessels is to be preferred. Further, a tool is preferred which in contradistinction to a spoon helps to avoid spillage of material on its way from where the sample is taken out to the test vessel.

The purpose of this invention is to provide a powder 25 pipette for taking out samples of a pulverulent material, which pipette is suited for being used in an automatic sampler taking out a sample of a powdery product and placing it in a test ves¬ sel and thereafter disposing of the used pipette and taking a new one from a storage for new and unused pipettes. Such a pi- 30 pette has to be simple, cheap and easy to handle, and it must ensure that the sample is representative for the product sampled, and that approximately the same quantity of material is taken out at each sampling.

This is obtained by a pipette which according to the 35 invention comprises a tube having an upper part integral with

a downward tapering lower part, the bottom of which is closed, the tapering lower part being split into at least two sections along planes parallel with the length axis of the pipette, the walls of the sections being provided with through-going notches and with means for opening and closing the pipette along the edges of the sections. Preferably, the lower tapering part is split into two sections along a plane through the axis of the pipette.

The closed pipette is stuck into the body of material to be sampled and is moved forwards and backwards to make material flow through the notches into the tapering interior of the tube. When the pipette is drawn out of the material and shaken, material lying above the notches flows out so that a well defined quantity of material is held by the pipette and may be transferred to a testtube or the like, where the pipette is opened to discharge its content. Thereafter the pipette is disposed of.

According to the invention the notches may be down¬ ward delimited by a horizontal plane cut to make more precise the level defined by the notches.

The horizontal edges of the notches may appropriately be sharpened so that no material can settle on these edges.

The pipette is opened and closed along the edges of the sections of the lower tapering part, and to avoid that ma- terial jamming at the end of the cuts causes leaking along the rest of the cut it is appropriate that the upper end of each axial cut splitting the lower parts is terminated by an opening in the tube wall.

According to the invention the pipette may be moulded from a plastic material, and the spring effect of the plastic material acts to keep the pipette open when not influenced. This is obtained by moulding the pipette in its open position. The closing of the pipette is then obtained by pres¬ sing the sections of the split lower part against each other against the resiliency of the plastic material. In preparation for this the pipette comprises constructions added to each sec-

tion of the split lower part, which constructions present even in the closed position of the pipette an upward tapering mainly conic surface coaxial with the pipette. These constructions are designed to cooperate with a tool on a robot arm, but may also cooperate with a manually operated tool or act as finger grips if the pipette is used manually.

The same way the upper part of the pipette may have a socket for receiving a gripping device of a robot. This soc¬ ket may simply be a piece of the upper part, into which a cor- responding cylindric rod on the robot fits when slightly pressed into its bore. To limit the insertion depth of the rod the socket may have an abutment at its inner side some distance away from the upper edge of the cylindric part.

According to an embodiment of the invention the pi- pette may also be at its upper edge provided with gripping fin¬ gers having protrusions cooperating with recesses in the grip¬ ping device of the tool.

The invention also relates to a tool for handling such a pipette. Such a tool comprises a gripping device for taking the pipette from a storage, an opening and closing devi¬ ce for closing the pipette when stuck into the material to be sampled and to open it when the material should be discharged, and an ejecting device to knock off the used pipette.

The gripping device may be a rod shaped member enga- ging the upper end of the pipette either by fitting narrowly into this end or by having a recess engaged by protrusions on fingers at the upper end of the pipette.

The opening and closing device may be a tube with a downward flaring bore within which tube the gripping rod may be axially displaced to bring the opening and closing means of the pipette out of and into contact with the inner surface of the downward flaring bore to make the sections of the pipette straddle away from each other and to press the sections toget¬ her, respectively. The ejecting device may be a tubular member slidingly fitting over the gripping device and being axially displaceable

along this device. When displaced in the direction toward the pipette the edge of the tubular ejecting member abuts the upper edge of the pipette mounted on the gripping device and further axial displacement of the ejecting member will knock off the pipette from the gripping device.

The tool may be designed as a manually operated tool comprising a handle firmly connected with the opening and clos¬ ing device and having a push button, the movement of which will first be transmitted to the gripping device to move this device relative to the opening and closing device and thereafter to the ejecting device to move this device relative to the grip¬ ping device.

Finally, it may be appropriate to provide the tool with an active shaking device either shaking the whole tool or only the gripping device. Such an active shaking device may be of any known kind and may be built into the handle of the tool or into the gripping device.

In the following an embodiment of the invention is described with reference to the drawings, wherein Fig. 1 shows a side view of an open pipette according to the invention. Fig. 2 shows a plane view of the pipette of Fig.

1, Fig. 3 shows a sectional front view of the pipette of Fig. 1,

Fig. 4 corresponds to Fig. 1 with the pipette closed. Fig. 5 shows a sectional view of the pipette of

Fig. 1 mounted in a robot tool. Fig. 6 shows a front sectional view of a manually operated tool handling a pipette according to the invention. Fig. 7 shows a sectional side view of the tool of

Fig. 6, and

Fig. 8 shows an adapting device to provide a pipette with gripping fingers at its upper end.

The pipette shown in Figures 1-4 comprises, as it is best seen in Fig. 3, an upper cylindric part 1 and a lower tapering part 2 increasingly tapering towards its lower closed end. The pipette is moulded from plastic material as one integral piece.

As seen in the closed position of the pipette as in Fig. 4, the lower tapering part 2 is split in two sections along a plane through the longitudinal axis of the pipette. The splitting is upwardly terminated by an opening 3 to avoid that jamming between the two sections should hamper the closing of the pipette. Further, the opening 3 defines a fulcrum when the spring effect of the plastic material is utilized as will be explained below.

The sections of the tapering part are provided with notches 4 at a chosen distance above the bottom of this part. The choice is made in accordance with the wanted quantity of material in the sample. This way this quantity may be varied within certain limits by altering the position of the notches. Further variation of the quantity may be obtained by choosing another diameter of the tube. To obtain a well defined level of material in the pipette the notches are downward limited by a plane horizontal cut. The horizontal edges formed by this cut leave surfaces on which material may settle. Therefore, such edges should be sharpened as shown in Figure 5.

The shown pipette is moulded from a plastic material in the position shown in Fig. 1. When a sample shall be taken the straddling sections of the lower part are pressed against each other to make a tight tapering tube with a closed bottom. The pipette is stuck into the material to be sampled and is moved forwards and backwards in the direction of the notches to make the powdery material flow in through the notches to fill the tube. When lifted out of the material body excessive material flows out of the notches, and by shaking the pipette

the level of material is limited to the level of the lower horizontal edge of the notches.

The pipette is now passed to the vessel intended to receive the sample and the pressure pressing the sections against each other is relieved. Now the sections will return to their straddling position, and the filling in the pipette will fall out into the receiving vessel possibly helped by snaking the pipette, which is thereafter thrown away. By being tapered the pipette may be stuck into the material body without influ- encing the grain distribution of the material adjacent to the pipette, and consequently a representative sample is ensured. In preparation of pressing the straddling sections against each other these sections may be provided with con¬ structions 5 providing a part of an upward tapering mainly co- nic surface coaxial with the pipette. These constructions are intended for the action of a tool, but may also act as finger grips if the pipette is used manually.

To provide a socket for a gripping device on a robot arm the bore of the upper cylindric part has at its upper end a slightly enlarged diameter. By the passage to the part of the bore having the normal diameter there is created a shoulder 6 serving as a stop for an inserted gripping tool, which may be a cylindric rod narrowly fitting into the enlarged diameter.

Fig. 5 shows the pipette mounted in a robot tool. The pipette is gripped from a storage by inserting the rod 7 in the part with the enlarged diameter. Thereafter a sleeve 8 with a conic bore is passed downwards to engage with the constructions 5 and further downwards to press the straddling sections against each other to close the pipette, which is then positio- ned above the material body to be sampled. The pipette is then lowered into the material body and moved to fill the pipette. Thereafter it is drawn out of the material body, shaken and then passed to the receiving vessel. The pipette is now opened by passing the sleeve 8 upwards out of engagement with the con- structions 5. The pipette is shaken to make sure that the ma¬ terial leaves the pipette, and thereafter the pipette is passed

to a position above a litter box. Now a sleeve 9 is passed downwards to knock the pipette off the rod 7, whereafter the sleeve 9 is passed back, and the robot is ready for a new cycle. Figures 6 and 7 show a tool for manual use of the pipette. This tool comprises a housing forming a handle 10 hav¬ ing at its upper end a protrusion 11 designed for resting on the fingers when the handle 10 is gripped by a hand. At its lower end the handle is provided with a tubular member 12 having a bore which continues up through the handle and which contains the functional elements of the tool. At its end op¬ posite the handle the bore is slightly flaring to engage the constructions 5 of a pipette.

The diameter of the bore varies in steps forming one shoulder inside the tubular member 12 and another inside the handle 10. Fitting into the bore a sleeve 13 rests on the shoulder in the tubular member. A rod 16, forming at its lower end a gripping device 14, is surrounded by a tubular member 15 extending from just above the gripping device 14 at one end of the rod 16 to a distance beyond the other end of the rod 16.

A helical spring 20 surrounding the rod 16 and the tubular member is held slightly compressed between an upper edge of the sleeve 13 and a pin 17 through the rod perpendicu¬ lar to its axis and projecting through slots 18 in the tubular member 15 into guiding slots 19 in the walls of the handle 10. Another spring 21 inside the tubular member 15 is slightly com¬ pressed between the upper end of the rod 16 and a push button 22 mounted at the upper end of the handle by a bushing 23 secured in this handle by a pair of screws 24. The hand tool described is designed to be used with pipettes having gripping fingers at their upper edge. Such gripping fingers may be casted integral with the pipette or they may be provided by fitting into the upper end of the pi¬ pette a gripping device as shown in figure 8. The device mentioned simply comprises a short cylin¬ dric part 25 which may be secured to the upper end of the pi-

pette by being press fitted, glued, or welded into this end. Along its edge the cylindric part is provided with spaced fin¬ gers 26 having at their outer ends protrusions 27 which may engage a recess 28 in the gripping device of a tool. When the tool in figures 6 and 7 is passed down over the end of a pipette stored in vertical position with its ta¬ pered end down, the upper end of the pipette passes into the bore of the tubular member 12. When the gripping device 14 rea¬ ches the gripping fingers 26 of the pipette these fingers are pressed outwards when their protrusions 27 ride over the grip¬ ping device 12. Thereby the upper edges of the fingers 26 will abut the lower edge of the sleeve 13 and when the pipette is passed further into the tool the sleeve 13 will be lifted from the shoulder in the tubular member 12 against the force of the spring 20. When the protrusions 27 on the fingers 26 of the pi¬ pette at last snap into the annular recess 28 in the rod 16 just above the gripping device 14 the sleeve will return to its shoulder abutting position and will now surround the outer end of the fingers preventing them from being forced out of engage- ment with the gripping device 14. The position of the gripping device 14 relative to the outer end of the tubular member 12 is so chosen that the sections of the pipette are closed by the flared bore of the tubular member 13 engaging the constructions 5 of the pipette when the pipette is gripped in the tool as described above.

The pipette may now be filled with powder by inser¬ ting it into the material body to be sampled. The opening of the pipette when the material should be discharged is obtained by pressing the push button 22. The movement of the push button 22 is transmitted via the spring 21 to the rod 16, and by the spring 21 being much stiffer than the spring 20 the spring 21 initially will act as a rigid connection so that the movement of the button 22 is transmitted to the rod 16, which against the force of the spring 20 will be moved forward and will move the pipette out of the bore of the tubular member 12. Thereby the constructions 5 of the pipette come out of engagement with

the flared opening of the tubular member 12 and the spring force of the pipette sections will move them away from each other opening the pipette.

If the button 22 is pushed further the pin 17 through the rod 16 will reach the bottom of the slots 19 in the handle and the forward movement of the rod will be stopped. Hereafter the spring 21 will be compressed and the push button will abut the end of the tubular member 15 and displace this member in relation to the rod 16. Thereby the other end of the tubular member 15 will abut the upper edges of the gripping fingers 27 and as the gripping device has been pushed forward, these fin¬ gers are no longer locked by the sleeve 13 and the movement of the tubular member 15 relative to the rod 16 will knock off the pipette. The manually operated tool may contain a kind of an active shaking mechanism to shake off excess material. This mechanism may with its power supply be accommodated in the handle or the mechanism may be accommodated in the rod 16 and the power supply in the handle. The shaking mechanism may be provided in the form of a piezo electric device or as a mechan¬ ical device with an unbalanced rotated part.

Another way to prevent settling of excess material is to omit horizontal surfaces, e.g. by letting the walls of the pipette taper to form a sharp edge at the lover end of the not- ches.

The pipette is here described as straddling in its neutral position. Of course, an embodiment according to which the pipette is closed in its neutral position and has means for opening it will be within the scope of the invention, just as the pipette may be used manually instead of with a tool. Alt¬ hough mainly described for taking out samples of a pulverulent product, the pipette may be used in all cases where apportioned quantities of powdery material shall be provided.