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Patent Searching and Data


Title:
PREPARATION METHOD FOR S-INDOXACARB
Document Type and Number:
WIPO Patent Application WO/2019/233209
Kind Code:
A1
Abstract:
A catalyst and a method for preparing S-indoxacarb using the catalyst. The catalyst is prepared using 3-tert-butyl-5-chloromethyl salicylaldehyde and cyclohexanediamine as raw materials, where an original quinine catalyst such as cinchonine is replaced with the catalyst for application in the asymmetric synthesis of tert-butyl hydroperoxide and 5-chloro-2-methoxycarbonyl-1-indanone ester, greatly improving selection in the asymmetric synthesis process, with the S-enantiomer content increasing from 75% to over 98%, achieving the recycling of a high-efficiency chiral catalyst, and greatly reducing production costs. The synthesis process of the catalyst is simple and is favorable for industrialization, and lays good foundations for the production of high-quality indoxacarb.

Inventors:
BO LEIFANG (CN)
CHENG DAOQUAN (CN)
LIU JIANCHENG (CN)
FENG PEILIANG (CN)
LIU HUAMIN (CN)
WANG ZHONGYANG (CN)
Application Number:
PCT/CN2019/084224
Publication Date:
December 12, 2019
Filing Date:
April 25, 2019
Export Citation:
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Assignee:
JINGBO AGROCHEMICALS TECH CO LTD (CN)
International Classes:
B01J31/22; C07B53/00; C07D237/04; C08G12/40
Foreign References:
CN101062903A2007-10-31
CN1630555A2005-06-22
CN106397351A2017-02-15
Other References:
See also references of EP 3804853A4
Attorney, Agent or Firm:
JINAN SHUNYUAN PATENT AGENCY CO., LTD. (CN)
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