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Title:
SELECTIVE ELECTROCHEMICAL DEPOSITION METHOD FOR NANO-SCALE PRUSSIAN BLUE THIN FILM
Document Type and Number:
WIPO Patent Application WO/2019/072034
Kind Code:
A1
Abstract:
A selective electrochemical deposition method for a nano-scale Prussian blue thin film, comprising: firstly preparing a metal electrode, the metal electrode comprising a pattern of a sensor working electrode and a pattern of a sensor counter electrode; subjecting the metal electrode to surface treatment to prepare a nanoscale or micron-scale surface microstructure; insulating the pattern of the sensor working electrode from the pattern of the sensor counter electrode; performing electrochemical deposition on the pattern of the sensor working electrode, and obtaining a Prussian blue thin film on the pattern of the sensor working electrode by controlling the deposition time, so as to form the sensor working electrode; and then performing stability scanning, heating, activation treatment and cleaning to obtain the sensor working electrode having a nanoscale Prussian blue thin film. The present invention performs surface treatment on the metal electrode to prepare a nano-scale or micron-scale surface microstructure, and improves the efficiency and effect of electrochemical deposition of Prussian blue.

Inventors:
FENG XUE (CN)
CHEN YIHAO (CN)
LU BINGWEI (CN)
Application Number:
PCT/CN2018/102439
Publication Date:
April 18, 2019
Filing Date:
August 27, 2018
Export Citation:
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Assignee:
UNIV TSINGHUA (CN)
International Classes:
G01N27/327; C25D9/02
Foreign References:
CN107860804A2018-03-30
CN107727723A2018-02-23
CN101024483A2007-08-29
Other References:
YANG, JIAO ET AL.: "Determination of Hydrogen Peroxide Using a Prussian Blue Modified Macroporous Gold Electrode", MIKROCHIMICA ACTA, vol. 182, no. 5-6, 31 December 2015 (2015-12-31), pages 1089 - 1094, XP055567125
Attorney, Agent or Firm:
BEIJING WANXIANGXINYUE INTELLECTUAL PROPERTY OFFICE (CN)
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