Title:
SINGLE-CRYSTAL X-RAY STRUCTURAL ANALYSIS DEVICE AND SAMPLE HOLDER MOUNTING DEVICE
Document Type and Number:
WIPO Patent Application WO/2020/105720
Kind Code:
A1
Abstract:
Provided are: a single-crystal X-ray structural analysis device and a sample holder mounting device that surely and easily enable work of detaching a sample occluded in a crystal sponge and work of loading of the sample to the structural analysis device. This sample holder mounting device is for mounting a sample holder that holds a sample to a single-crystal X-ray structural analysis device for performing structural analysis of a substance. The sample holder mounting device is provided with a sample holder mounting mechanism 600 that mounts a sample holder 250 to a goniometer 12 of the single-crystal X-ray structural analysis device, the sample holder 250 being provided in a form of being attached to an attachable/detachable applicator 300 but being detached from the applicator 300 for the mounting. The sample holder 250 includes a porous complex crystal capable of occluding the sample in a plurality of micropores formed inside. In a state where the sample holder 250 is mounted to the goniometer 12, the porous complex crystal is fixed to a position of the sample holder 250 where X rays from the X-ray irradiation unit are emitted.
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Inventors:
SATO TAKASHI
Application Number:
PCT/JP2019/045689
Publication Date:
May 28, 2020
Filing Date:
November 21, 2019
Export Citation:
Assignee:
RIGAKU DENKI CO LTD (JP)
International Classes:
G01N23/20025; G01N23/207
Domestic Patent References:
| WO2014038220A1 | 2014-03-13 | |||
| WO2016017770A1 | 2016-02-04 |
Foreign References:
| US20050163280A1 | 2005-07-28 | |||
| JP2018155680A | 2018-10-04 | |||
| JPH11304999A | 1999-11-05 | |||
| JP2010203843A | 2010-09-16 | |||
| JP2010286431A | 2010-12-24 | |||
| US20110211674A1 | 2011-09-01 | |||
| US7660389B1 | 2010-02-09 | |||
| JP2003139726A | 2003-05-14 | |||
| JP2007003394A | 2007-01-11 | |||
| JP2018218756A | 2018-11-22 |
Other References:
"X-ray analysis on the nanogram to microgram scale using porous complexes", NATURE, vol. 495, 28 March 2013 (2013-03-28), pages 461 - 466, XP055400439
MASAHIKO HIRAKI: "RSJ2014AC1Q3-01: Development of sample exchange system for synchrotron radiation beamline", ANNUAL CONFERENCE OF THE ROBOTICS SOCIETY OF JAPAN , vol. 32, no. 1, 4 September 2014 (2014-09-04), JP, pages 1 - 2, XP009521330
TAKATA MASAKI: "New Nano Science for one-dimensional arrays of dioxygen", SPRING-8 INFORMATION, vol. 8, no. 6, November 2003 (2003-11-01), pages 406 - 412, XP009521329, ISSN: 2187-4794
"Direct observation of hydrogen molecules adsorbed in a microporous coordination polymer", SPRING-8 INFORMATION, vol. 10, no. 1, January 2005 (2005-01-01), pages 24 - 29, XP001236796
KUROIWA, YOSHIHIRO: "Study on precise structural properties by powder crystal", SPRING-8 RIYOSHA JOHO - SPRING-8 INFORMATION, SPRING-8 RIYOSHA JOHO HENSHU IINKAI, KAMIGORI-CHO, JP, vol. 11, no. 4, 30 June 2006 (2006-06-30), JP, pages 202 - 219, XP009528339, ISSN: 1341-9668
TAKATA, MASAKI; KATO, KEN-ICHI: "Precise structural studies for novel materials science by synchrotron radiation powder diffraction", JSAP INTERNATIONAL, vol. 74, no. 9, 31 August 2005 (2005-08-31), JP, pages 1201 - 1204, XP009528328, ISSN: 0369-8009, DOI: 10.11470/oubutsu.74.9_1201
MAKOTO FUJITA: "X-ray analysis on the nanogram to microgram scale using porous complexes", NATURE, vol. 495, 28 March 2013 (2013-03-28), pages 461 - 466, XP055400439, DOI: 10.1038/nature11990
HOSHINO ET AL., THE UPDATED CRYSTALLINE SPONGE METHOD IUCRJ, vol. 3, 2016, pages 139 - 151
See also references of EP 3885749A4
MASAHIKO HIRAKI: "RSJ2014AC1Q3-01: Development of sample exchange system for synchrotron radiation beamline", ANNUAL CONFERENCE OF THE ROBOTICS SOCIETY OF JAPAN , vol. 32, no. 1, 4 September 2014 (2014-09-04), JP, pages 1 - 2, XP009521330
TAKATA MASAKI: "New Nano Science for one-dimensional arrays of dioxygen", SPRING-8 INFORMATION, vol. 8, no. 6, November 2003 (2003-11-01), pages 406 - 412, XP009521329, ISSN: 2187-4794
"Direct observation of hydrogen molecules adsorbed in a microporous coordination polymer", SPRING-8 INFORMATION, vol. 10, no. 1, January 2005 (2005-01-01), pages 24 - 29, XP001236796
KUROIWA, YOSHIHIRO: "Study on precise structural properties by powder crystal", SPRING-8 RIYOSHA JOHO - SPRING-8 INFORMATION, SPRING-8 RIYOSHA JOHO HENSHU IINKAI, KAMIGORI-CHO, JP, vol. 11, no. 4, 30 June 2006 (2006-06-30), JP, pages 202 - 219, XP009528339, ISSN: 1341-9668
TAKATA, MASAKI; KATO, KEN-ICHI: "Precise structural studies for novel materials science by synchrotron radiation powder diffraction", JSAP INTERNATIONAL, vol. 74, no. 9, 31 August 2005 (2005-08-31), JP, pages 1201 - 1204, XP009528328, ISSN: 0369-8009, DOI: 10.11470/oubutsu.74.9_1201
MAKOTO FUJITA: "X-ray analysis on the nanogram to microgram scale using porous complexes", NATURE, vol. 495, 28 March 2013 (2013-03-28), pages 461 - 466, XP055400439, DOI: 10.1038/nature11990
HOSHINO ET AL., THE UPDATED CRYSTALLINE SPONGE METHOD IUCRJ, vol. 3, 2016, pages 139 - 151
See also references of EP 3885749A4
Attorney, Agent or Firm:
FUKUCHI Takeo (JP)
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