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Title:
フルオロアルキルアイオダイドおよびその製造方法
Document Type and Number:
Japanese Patent JP4802544
Kind Code:
B2
Abstract:
A process for producing a fluoroalkyl iodide as a telomer R f (CF 2 CF 2 ) n I (wherein R f is a C 1-10 fluoroalkyl group, and n is an integer of from 1 to 6) by telomerization from a fluoroalkyl iodide represented by the formula R f I (wherein R f is as defined above) as a telogen and tetrafluoroethylene (CF 2 CF 2 ) as a taxogen, which comprises a liquid phase telomerization step of supplying a homogeneous liquid mixture of the telogen and the taxogen from the lower portion of a tubular reactor, moving the mixture from the lower portion towards the upper portion of the reactor in the presence of a radical initiator over a retention time of at least 5 minutes while the reaction system is kept in a liquid phase state under conditions where no gas-liquid separation will take place, so that the taxogen supplied to the reactor is substantially consumed by the reaction in the reactor, and drawing the reaction product from the upper portion of the reactor.

Inventors:
Noboru Furuta
Yusuke Sugawara
Keiko Nakase
Keisuke Mori
Application Number:
JP2005122286A
Publication Date:
October 26, 2011
Filing Date:
April 20, 2005
Export Citation:
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Assignee:
Asahi Glass Co., Ltd.
International Classes:
C07C17/278; C07C19/16
Domestic Patent References:
JP2002316957A
JP10059880A
JP6206908A
JP8252453A
Attorney, Agent or Firm:
Nozomi Watanabe
Haruko Sanwa