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Title:
METHOD FOR PREPARING CHEMILUMINESCENT HYDROGEL
Document Type and Number:
WIPO Patent Application WO/2022/032714
Kind Code:
A1
Abstract:
A method for preparing a chemiluminescent hydrogel, belonging to the field of luminescent materials. The method for preparing a luminescent hydrogel comprises: slowly adding chitosan to an acetic acid solution, stirring same at room temperature until the chitosan is completely dissolved, then adding a cobalt chloride solution, followed by a polyvinyl alcohol solution, sufficiently stirring same, then ultrasonically defoaming same, and subjecting same to an alkaline bath treatment with an alkaline solution and adding N-(4-aminobutyl)-N-ethylisoluminol (ABEI), stirring same, and then adding a hydrogen peroxide solution to obtain chemiluminescent hydrogel. The synthesized hydrogel has the advantages of high luminous intensity, being long-lasting, etc. In the process, a high-water-content polymer with a three-dimensional network structure obtained by means of chemical crosslinking with the addition of polyvinyl alcohol has the characteristics of good biocompatibility, high elasticity, being non-toxic, etc., and is also one of biomedical materials with application potential.

Inventors:
MA JILIANG (CN)
SUN RUNCANG (CN)
JIN DONGNV (CN)
Application Number:
PCT/CN2020/110495
Publication Date:
February 17, 2022
Filing Date:
August 21, 2020
Export Citation:
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Assignee:
UNIV DALIAN POLYTECHNIC (CN)
International Classes:
C08J3/075; C09K11/07; C08L5/08; C08L29/04
Foreign References:
CN106833618A2017-06-13
CN106279724A2017-01-04
CN111234266A2020-06-05
CN105968388A2016-09-28
CN103601904A2014-02-26
Other References:
BAI TONGCHUN, CHEN XINGBO, WANG NA, WANG YUANYUAN: "The Physical-Chemistry Properties of Poly(vinyl alcohol)/Chitosan Composite Hydrogels", ZHONGGUO KEXUE. HUAXUE - SCIENTIA SINICA CHIMICA, ZHONGGUO KEXUE ZAZHISHE, CN, vol. 44, no. 10, 20 October 2014 (2014-10-20), CN , pages 1591 - 1598, XP055899926, ISSN: 1674-7224, DOI: 10.1360/N032013-00086
JIANG LEI, LIN BAOFENG, LIANG XINGQUAN, LIU SIQIAN: "Progress in the Research of Hydrogels of Chitosan and its Derivatives", HUA HSUEH TUNG PAO - CHEMICAL BULLETIN, ZHONGGUO KEXUEYUAN HUAXUE YANJIUSUO, CN, no. 1, 18 January 2007 (2007-01-18), CN , pages 47 - 51, XP055899930, ISSN: 0441-3776, DOI: 10.14159/j.cnki.0441-3776.2007.01.008
Attorney, Agent or Firm:
DALIAN EAST PATENT AGENT LTD. (CN)
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