Title:
METHOD FOR PRODUCING (2-METHOXYETHYL) VINYL ETHER, AND METHOD FOR REFINING (2-METHOXYETHYL) VINYL ETHER
Document Type and Number:
WIPO Patent Application WO/2022/168950
Kind Code:
A1
Abstract:
Provided is a method for producing a (2-methoxyethyl) vinyl ether at a high level of purity from 2-methoxyethanol and acetylene. A method for producing a (2-methoxyethyl) vinyl ether that treats 2-methoxyethanol as a source material alcohol, and includes the following steps A1, A2, and A3. (Step A1) A vinyl ether synthesis step in which 2-methoxyethanol and acetylene are reacted to obtain a mixture that includes unreacted 2-methoxyethanol and the (2-methoxyethyl) vinyl ether. (Step A2) An acetalization step in which the unreacted 2-methoxyethanol and the (2-methoxyethyl) vinyl ether in the mixture are reacted in the presence of an acid catalyst and converted into acetaldehyde bis(2-methoxyethyl) acetal. (Step A3) A distillation step in which distillation is used to remove the acetaldehyde bis(2-methoxyethyl) acetal from the acetal-including mixture that was obtained in step A2.
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Inventors:
TENJINBAYASHI RYUICHI (JP)
SAITO KYOHEI (JP)
ITO YUDAI (JP)
NANIKI TAKASHI (JP)
SATO TOMOHIKO (JP)
SAITO KYOHEI (JP)
ITO YUDAI (JP)
NANIKI TAKASHI (JP)
SATO TOMOHIKO (JP)
Application Number:
PCT/JP2022/004490
Publication Date:
August 11, 2022
Filing Date:
February 04, 2022
Export Citation:
Assignee:
MARUZEN PETROCHEM CO LTD (JP)
International Classes:
C07C41/30; C07C41/42; C07C43/16; C07B61/00
Domestic Patent References:
WO2018051996A1 | 2018-03-22 |
Foreign References:
JP2018058798A | 2018-04-12 | |||
JP2010229049A | 2010-10-14 | |||
CN101898939A | 2010-12-01 | |||
JP5312133B2 | 2013-10-09 | |||
JP2019044050A | 2019-03-22 | |||
JPH08268945A | 1996-10-15 | |||
DE1957680A1 | 1971-05-19 | |||
JPS4876803A | 1973-10-16 | |||
JPH08277237A | 1996-10-22 |
Other References:
J.ORG.CHEM., vol. 38, 1973, pages 2910
HELV.CHIM.ACTA, vol. 1158, 1967
BULL.CHEM.SOC.JPN, vol. 3089, 1976
HELV.CHIM.ACTA, vol. 1158, 1967
BULL.CHEM.SOC.JPN, vol. 3089, 1976
Attorney, Agent or Firm:
THE PATENT CORPORATE BODY ARUGA PATENT OFFICE (JP)
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