Title:
METHOD FOR PRODUCING ACID HALIDE SOLUTION AND METHOD FOR PRODUCING MONOESTER COMPOUND
Document Type and Number:
WIPO Patent Application WO/2017/130871
Kind Code:
A1
Abstract:
The present invention provides a method for producing an acid halide solution that is useful when producing a polymerizable liquid crystal compound. This method for producing an acid halide solution includes: a first step of obtaining a reaction solution comprising a solution that contains an acid halide compound which is obtained by reacting a specific dicarboxylic acid compound with a halogenating agent in a water-immiscible organic solvent in the presence of an activator at a quantity of 1.1-3.0 equivalents relative to the dicarboxylic acid compound, and that contains an oily liquid which is immiscible with the solution containing the acid halide compound; and a second step of removing the oily liquid from the reaction solution obtained in the first step so as to obtain a purified solution that contains the acid halide compound.
Inventors:
SANUKI KANAKO (JP)
SAKAMOTO KEI (JP)
OKUYAMA KUMI (JP)
IWAKI HIROKI (JP)
SAKAMOTO KEI (JP)
OKUYAMA KUMI (JP)
IWAKI HIROKI (JP)
Application Number:
PCT/JP2017/002024
Publication Date:
August 03, 2017
Filing Date:
January 20, 2017
Export Citation:
Assignee:
ZEON CORP (JP)
International Classes:
C07C51/60; C07C61/09; C07C67/14; C07C69/75; C07B61/00
Domestic Patent References:
| WO2016002816A1 | 2016-01-07 | |||
| WO2016159193A1 | 2016-10-06 |
Foreign References:
| JP2013018714A | 2013-01-31 |
Other References:
KENNETH A. BURDETT ET AL.: "An Improved Acid Chloride Preparation via Phase Transfer Catalysis", SYNTHESIS, 1991, pages 441 - 442, XP002630856, ISSN: 0039-7881
See also references of EP 3409657A4
See also references of EP 3409657A4
Attorney, Agent or Firm:
SUGIMURA Kenji (JP)
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