Title:
METHOD FOR PRODUCING FLUORINE-CONTAINING (CYCLO)ALKENYL ZINC HALIDE COMPOUND
Document Type and Number:
WIPO Patent Application WO/2021/132011
Kind Code:
A1
Abstract:
According to the present invention, a fluorine-containing (cyclo)alkenyl zinc halide compound is able to be obtained with a high yield by reacting a halogenated olefin compound represented by general formula (2) (wherein R1, R2 and R3 are as defined above; X2 represents a halogen atom; and a single bond denoted by a wiggly line indicates that the steric configuration of a double bond to which the single bond is bonded is E configuration, Z configuration or a mixture thereof at an arbitrary ratio) and a zinc halide compound represented by formula (3) ZnX1 (wherein X1 is as defined above) with each other in the presence of a zero-valent alkali metal.
Inventors:
ETOU YUUSUKE (JP)
ADACHI KENJI (JP)
OGOSHI SENSUKE (JP)
ADACHI KENJI (JP)
OGOSHI SENSUKE (JP)
Application Number:
PCT/JP2020/047128
Publication Date:
July 01, 2021
Filing Date:
December 17, 2020
Export Citation:
Assignee:
DAIKIN IND LTD (JP)
UNIV OSAKA (JP)
UNIV OSAKA (JP)
International Classes:
C07F3/06; B01J23/04; C07B61/00; C07C17/26; C07C21/18
Domestic Patent References:
| WO2013172337A1 | 2013-11-21 | |||
| WO2019151467A1 | 2019-08-08 |
Foreign References:
| JPH08505440A | 1996-06-11 | |||
| JP2016128415A | 2016-07-14 |
Other References:
OPPOLZER, WOLFGANG ET AL.: "ENANTIOSELECTIVE ADDITION OF (Z)- AND (E)-ALKENYLZINC BROMIDES TO ALDEHYDES: ASYMMETRIC SYNTHESIS OF SEC- ALLYLALCOHOLS", TETRAHEDRON LETTERS, vol. 32, no. 41, 1991, pages 5777 - 5780, ISSN: 0040-4039
Attorney, Agent or Firm:
SAEGUSA & PARTNERS (JP)
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