FIELD OF THE DISCLOSURE:

The present disclosure relates to a process for the preparation of herbal cosmeceutical compositions. The present disclosure particularly relates to a process for the preparation of preservative free herbal cosmeceutical compositions.

BACKGROUND:

Cosmeceuticals are cosmetic products with biologically active ingredients purporting to have medicinal or drug-like benefits. In other words, a cosmeceutical is a substance with medicinal properties that manifests beneficial topical actions and provides protection against degenerative skin conditions.

Among the various applications, cosmeceuticals can be effectively used for the nourishment and hydration of the skin and also for avoiding and curing various dermatological conditions. Cosmeceutical preparations, especially those comprising herbal ingredients, have been enjoying an ever increasing popularity with consumers.

Herbal drugs or actives have been used since ancient times for different purposes including medicinal and beautification purposes. They have been used in both fresh as well as dried form. Herbal preparations are unique, in that, the herbs may be used by including then in some preparation or by directly applying to the body, with or without the use of additives. However, now-a-days extracts of herbs obtained by various extraction methods such as decoction, infusion, steam distillates, soxhlet extraction and the like are also being used in cosmeceutical formulations rather than the herbs themselves. This necessitates the inclusion of preservatives in the formulations for prolonging their shelf-life. The use of preservatives such as parabens and formaldehyde donating species may, however, elicit allergenic responses in certain users, thereby restricting the consumption of these preparations. There is therefore a need to develop effective processes and products, devoid of preservatives, that may be used for cosmeceutical applications.

OBJECTS: It is an object of the present disclosure to provide a process for the preparation of preservative free herbal cosmeceutical compositions.

It is another object of the present disclosure to provide preservative free herbal cosmeceutical compositions.

It is still another object of the present disclosure to provide preservative free herbal cosmeceutical compositions with synergistic effects.

It is yet another object of the present disclosure to provide preservative free herbal cosmeceutical compositions which are safe and free from toxic materials.

It is still another object of the present disclosure to provide preservative free herbal cosmeceutical compositions which are cost effective.

Other objects and advantages of the present disclosure will be more apparent from the following description, which are not intended to limit the scope of the present disclosure. SUMMARY:

In accordance with one aspect of the present disclosure there is provided a process for preparing a preservative free herbal cosmeceutical composition, said process comprising:

a. obtaining at least one substance derived from at least one botanical, selected from the group consisting of Aloe barbadensis, Rosa sinensis, Emblica officinalis, Eclipta alba, Lawsonia inermis, Curcuma longa and Cucumis sativus, wherein the amount of the substance is in the range of 1% to 99% with respect to the total mass of the composition;

b. obtaining at least one excipient;

c. optionally, sterilizing the substances and the excipients;

d. mixing at least one substance and at least one excipient under aseptic conditions to obtain a herbal cosmeceutical composition;

e. filling the herbal cosmeceutical composition in a pre-sterilized packaging material under aseptic condition and subsequently sealing said packaging material to obtain a pack containing the preservative free herbal cosmeceutical composition; and

f. sterilizing the pack containing the preservative free herbal cosmeceutical composition.

Typically, the excipient is at least one selected from the group consisting of surfactants, emulsifiers, vehicles, gelling agents, oils, waxes, emollients, perfumes, coloring agents, propellants, opacifiers, humectants, antioxidants, suspending agents, penetration enhancers, thickening agents, antifoaming agents, scrub beads and plasticizers.

Typically, the excipient is at least one selected from the group consisting of carbomer, polyethylene glycol, cocamidopropyl betaine (CAPB), polysorbate 20, disodium EDTA, sodium hydroxide, glycerin and water.

the sterilization is carried out using at least one method selected from the group consisting of heat sterilization, steam sterilization, radiation sterilization and gaseous sterilization.

Typically, the sterilization comprises autoclaving at a temperature ranging between 11 °C and 130°C for a time period ranging between 30min. and 2hrs.

Typically, the sealing is carried out using at least one method selected from the group consisting of cold sealing, heat sealing, vacuum sealing and hermetic sealing.

Typically, the pack is selected from the group consisting of heat sealable pouch, tubes, sachets, pouches, vials, bottles, cans and tins.

Typically, said composition is in the form of gel, granules, powder, oil, solution, suspension, emulsion, paste, lotion, cream, ointment, aerosol and semisolid.

In accordance with another aspect of the present disclosure there is provided a preservative free herbal cosmeceutical composition, said composition comprising:

a. at least one substance derived from at least one botanical selected from the group consisting of Aloe barbadensis, Rosa sinensis, Emblica officinalis, Eclipta alba, Lawsonia inermis, Curcuma longa and Cucumis sativus, wherein the amount of the substance is in the range of 1% to 99% with respect to the total mass of the composition; and

b. at least one excipient selected from the group consisting of surfactants, emulsifiers, vehicles, gelling agents, oils, waxes, emollients, perfumes, coloring agents, propellants, opacifiers, humectants, antioxidants, suspending agents, penetration enhancers, thickening agents, antifoaming agents, scrub beads and plasticizers.

Typically, said composition is in the form of gel, granules, powder, oil, solution, suspension, emulsion, paste, lotion, cream, ointment, aerosol and semisolid.

Typically, the excipient is at least one selected from the group consisting of carbomer, polyethylene glycol, cocamidopropyl betaine (CAPB), polysorbate 20, disodium EDTA, sodium hydroxide, glycerin and water.

In accordance with yet another aspect of the present disclosure there is provided a pack containing preservative free herbal cosmeceutical composition Typically, the pack is selected from the group consisting of heat sealable pouch, tubes, sachets, pouches, vials, bottles, cans and tins.

DETAILED DESCRIPTION:

With the aim of obviating the problems associated with the use of preservatives, the inventors of the present disclosure have conducted several trials and experiments and have developed a process for the preparation of herbal cosmeceutical compositions that do not involve the use of preservatives. The absence of preservatives makes the preparation more tolerable and therefore more acceptable among the users. The herbal composition prepared by the aforementioned process typically contains one or more bioactive ingredients or extracts of botanicals.

In accordance with one aspect of the present disclosure, there is provided a process for the preparation of preservative free herbal cosmeceutical compositions.

In the first step, one or more substances derived from at least one botanicals, selected from the group consisting of Aloe barbadensis, Rosa sinensis, Emblica officinalis, Eclipta alba, Lawsonia inermis, Curcuma longa and Cucumis sativus are mixed with one or more excipient to obtain a cosmeceutical composition.

Typically, the amount of the substance is in the range of 1 % to 99% with respect to the total mass of the composition.

Typically, the excipient includes surfactants, emulsifiers, vehicles, gelling agents, oils, waxes, emollients, perfumes, coloring agents, propellants, opacifiers, humectants, antioxidants, suspending agents, penetration enhancers, thickening agents, antifoaming agents, scrub beads and plasticizers.

In the second step, the cosmeceutical composition is filled in a pre-sterilized packaging material under aseptic condition and subsequently the packaging material is sealed to obtain a pack containing the preservative free cosmeceutical composition.

In accordance with one embodiment of the present disclosure, a preservative free cosmeceutical composition is prepared by initially accurately weighing and sterilizing all the ingredients individually. Post-sterilization, the ingredients are admixed, in any sequence, under aseptic conditions, to obtain the preservative free cosmeceutical composition. This composition is then filled in pre-sterilized containers, under aseptic conditions, followed by sealing. Finally, the sealed containers are sterilized, and then packed, as required. Typically, the sterilization is carried out by any method selected from the group that includes but is not limited to heat sterilization, steam sterilization, radiation sterilization and gaseous sterilization.

In one embodiment, sterilization is carried out by autoclaving at a temperature ranging between 1 10 °C and 130 °C for a time period ranging between 30min and 2 hrs.

In accordance with a second embodiment of the present disclosure, a preservative free cosmeceutical composition is prepared by accurately weighing and admixing all the ingredients, in any sequence, to obtain the cosmeceutical composition. The resultant composition is then subjected to sterilization. The sterilized composition is further filled in pre-sterilized containers, under aseptic conditions, followed by sealing. Finally, the sealed containers are sterilized, and then packed.

In accordance with a third embodiment of the present disclosure, a preservative free cosmeceutical composition is prepared by accurately weighing and admixing all the ingredients, in any sequence, to obtain the herbal cosmeceutical composition. The resultant composition is then filled in pre-sterilized containers, followed by sealing. Finally, the sealed containers are sterilized, and then packed.

Typically, the sealing of the packaging material is carried out by using one or more methods selected from the group which includes cold sealing, heat sealing, vacuum sealing and hermetic sealing.

The composition of the present disclosure is in the form that includes but is not limited to gel, granules, powder, oil, solution, suspension, emulsion, paste, lotion, cream, ointment, aerosol and semisolid.

In accordance with an exemplary embodiment of the present disclosure, a preservative free cosmeceutical composition, in gel form, is prepared by dispersing carbomer in demineralized water followed by the addition of other'excipients and substances derived from botanicals, to obtain a dispersion. Further, sodium hydroxide is added to the dispersion, which converts the dispersion into gel from. The composition in the form of gel is subsequently filled into pre- sterilized containers and sealed. Finally, the sealed containers are autoclaved at a temperature ranging between 110 °C and 130 °C for a time period ranging between 30min. and 2 hrs.

The container includes but is not limited to sachets, pouches, vials, bottles, cans, tubes and tins. In one embodiment, the container may be a unit dose container, a unit dispensing device and the like. Aloe

Description: Aloe belongs to the Asphodelaceae (Liliaceae) family and is a shrubby or arborescent, perennial, xerophytic and succulent, pea- green color plant.

Synonym: Aloe barbadensis Miller, Aloe vera, Acibar, Ailwa, Airyo, Alo, Aloe Cactus, Aloe Indian, Aloe Elongata, Aloe indica Royle, Aloe perfoliate! L., A. vulgaris Lam and Aloes

Geographical source and distribution: Aloe is known to have originated in northern Africa, however, it is widely cultivated throughout the world. It is commonly found in the Arabian peninsula, North Africa (Morocco, Mauritania, Egypt) as well as Sudan and the other neighboring countries, along with the Canary, Cape Verde, and Madeira Islands. It is also found in India, Australia, Barbados, Belize, Nigeria, Paraguay and the United States of America.

Cultivation: Aloe vera is widely grown as an ornamental plant and its succulence allows the species to survive in areas of low rainfall. Upon cultivation in pots, the species requires well- drained sandy potting soil and bright sunny conditions. Chemical constituents: Acetylated mannans, aloins, polymannans, anthraquinone C-glycosides, anthrones, anthraquinones, such as emodin, and various lectins are the most common chemical constituents present in aloe.

Uses: The aloe plant may be used for a very diverse spectrum of applications such as a cooling and moisturizing agent, skin protection and anticancer agent, use in dental care, wound and lesion treatment, diabetes management, source of proteins, lipids, amino acids, vitamins, enzymes, inorganic and organic compounds and carbohydrates. Aloe has an extremely diverse sphere of applications with respect to skin care products. The mucopolysaccharides present in aloe help in binding moisture into the skin. Aloe stimulates fibroblasts which produces the collagen and elastin fibers making the skin more elastic and less wrinkled. It also has cohesive effects on the superficial flaking epidermal cells by sticking them together, thereby softening the skin. The amino acids also soften hardened skin cells and zinc acts as an astringent to tighten pores. Its moisturizing effects have also been studied in the treatment of dry skin which is associated with occupational exposure. Aloe vera gel gloves have shown improved skin integrity, decrease in the appearance of fine wrinkles and decrease in erythema. It has also shown anti-acne effect. Further, aloe vera gel has also been reported to have a protective effect against radiation damage to the skin. Post exposure to aloe vera gel, an antioxidant protein, metallothionein, is generated in the skin, which scavenges hydroxyl radicals and prevents suppression of superoxide dismutase and glutathione peroxidase in the skin. This reduces the production and release of skin keratinocyte-derived immunosuppressive cytokines such as interleukin-10 (IL-10) and hence prevents UV-induced suppression of delayed type hypersensitivity.

Amla

Description: Amla is a highly nutritious plant belonging to the family Phyllanthaceae.

Synonym: Emblica officinalis, emblic myrobalan, amalaki, Indian gooseberry, amalika, amla, amlaa, amlakhi, aavalaa, ma kham pom and anmole.

Geographical origin: Amla is widely distributed in most of the tropical and subtropical countries such as China, India, Indonesia, the Malay Peninsula and Southeast Asia. The species is native to India and grows in Pakistan, Uzbekistan, Sri Lanka and Bangladesh.

Cultivation: Amla is cultivated as an orchard crop in India, especially in the warmer, semi- arid coastal regions in India. With orchard-type cultivation, about 200 trees can be accommodated per acre. The tree ripens in autumn and bears fruit for up to 65 to 70 years and it is a common practice to harvest the berries by hand. About 5,000 to 10,000 kg of fruit per month is exported by India to Singapore, Malaysia and Europe.

Chemical constituents: Ascorbic acid (vitamin C), ellagitannins such as emblicanin A (37%), emblicanin B (33%), punigluconin (12%) and pedunculagin (14%), punicafolin, phyllanemblinin A, B, C, D, E and F and polyphenols such as flavonoids, kaempferol, ellagic acid and gallic acid are the common chemical constituents of Amla.

Uses: Amla is highly nutritious and is an important dietary source of minerals, amino acids and vitamins such as Vitamin C, thiamine, riboflavin and niacin. Traditionally, the fruit is useful as an astringent, cardiotonic, diuretic, laxative, liver tonic, refrigerant, stomachic, restorative, antipyretic, anti-inflammatory and hair tonic. Promotes longevity and prevents maladies of old age. Further, it helps to attain a state of enhanced well-being such as improving the memory and intellect. Even further, amla hastens recovery from disease. Haridra

Description: Haridra is a perennial herb with pulpy, orange, tuberous roots belonging to the family Zingiberaceae.

Synonyms: Curcuma longa, haldi, curcuma, halad, Curcuma rotunda and Amomum curcuma.

GeoRraphical origin: It is native to tropical South Asia. India, China, Pakistan Bangladesh and other Asian countries are the places where turmeric trees are commonly found.

Cultivation: Turmeric or haridra needs temperatures between 20 °C and 30 °C (68 °F and 86 °F) and a considerable amount of annual rainfall to grow and propagate. The rhizomes are gathered annually and used for a wide spectrum of applications. These rhizomes are in turn used for further propagation in the following season.

Chemical constituents: Curcumin, demethoxycurcumin, bisdemethoxycurcumin, turmerin, wenyujinlactone A, neolitamone A, zedoarondiol, isozedoarondiol, aerugidiol, curcumol, curdione, (lR,10R)-epoxy-(-)-l, 10- dihydrocurdine3 and parviflorene F4 are the common chemical constituents of haridra.

Uses: It has analgesic, anti-inflammatory, anti-blood clotting, antibacterial, expectorant and antioxidant activities. It is used for the treatment of diseases such as arthritis, gastrointestinal distress, dyspepsia, cognitive function disorders, gallstone, various types of inflammation, irritable bowel syndrome, osteoarthritis and viral infection.

Hibiscus

Description: Hibiscus is a bushy, evergreen shrub or small tree belonging to the family Malvaceae and has glossy leaves and solitary, brilliant red flowers that flower in summer and autumn. The 5-petalled flowers have characteristic orange-tipped red anthers.

Synonym: Rosa sinensis, rose mallow, Chinese hibiscus, China rose, shoe flower Jasvand, Shoe-Black and Shoe-back-plant.

Geographical origin: The plant is native to East Asia and is widely found in Egypt, Sudan, Mexico, Thailand, India and China. Cultivation: Hibiscus is widely grown as an ornamental plant throughout the tropical and subtropical regions. The plant does not tolerate temperatures below 10 °C (50 °F) and is therefore best grown in temperate regions under glass. The plant when cultivated in containers, may however, be placed outside during the summer months.

Chemical constituents: Hibiscus contains anthocyanins, flavonoids, cyanidin-3,5-diglucoside, cyanidin-3-sophoroside-5-glucoside, quercetin-3,7-diglucoside, quercetin-3-diglucoside, a cyclopeptide alkaloid, cyanidin chloride, quercetin, hentriacontane, and vitamins such as riboflavin, ascorbic acid and thiamine.

Uses: The plant has a very diverse spectrum of activities that include diuretic, demulcent, antidiarrheal, aphrodisiac, abortifacient and antitussive. It is also used for the management of conditions such as gonorrhea, irregular menstruation, flu & cough, stomach pain, eye problems, cough, fever and in labor. The leaves and flowers show exceptional hair growth and anti-greying properties.

Maka

Description: Maka is a small branched annual herbaceous plant belonging to the family Asteraceae.

Synonym: Eclipta alba Hassk, False Daisy, Eclipta prostrata, Bhringaraj and yerba de tago.

Geographical origin: Maka is a plant native to the U.S.A and the tropical areas worldwide. It is commonly found in India, China, Thailand, and Brazil.

Cultivation: This plant is quite prolific and can grow on land or directly in water. It grows commonly, as a weed, in moist places, in warm temperate to tropical areas in the world. It is a plant thriving throughout the year, however, is more commonly observed at the end of the rainy season and during winters. It prefers a clayey soil with abundant moisture. The germination percentage of seeds is 62% in diffused sunlight, whereas that in continuous light with pre-treatment of seeds with mud is higher.

Chemical constituents: Eclipta alba (L.) contains a wide variety of active principles which includes coumestans, alkaloids, flavonoids, glycosides, polyacetylenes, triterpenoids. The leaves contain stigmasterol, a-terthienylmethanol, wedelolactone, demethylwedelolactone and demethylwedelolactone-7-glucoside. The roots contain hentriacontanol and heptacosanol and polyacetylene substituted thiophenes. The aerial part is reported to contain a phytosterol, P-amyrin in the n-hexane extract and luteolin-7-glucoside, P-glucoside of phytosterol, a glucoside of a triterpenic acid and wedelolactone in polar solvent extract. The polypeptides isolated from the plant yield cystine, glutamic acid, phenyl alanine, tyrosine and methionine.

Uses: Maka is a powerful liver tonic, a rejuvenator and is especially good for the hair. It is effective when used on the scalp to manage hair loss. It is used for management of conditions such as athlete's foot, eczema and dermatitis. Roots of Eclipta prostrata are emetic and purgative. Black dye obtained from Eclipta prostrata is used for dyeing hair and tattooing and also as anti-venom against snake bite.

Henna

Description: Henna is a flowering plant and a sole species in the genus in the family Lythraceae.

Synonym: Lawsonia inermis, Lawsonia alba and hina

Geographical origin: Henna is native to tropical and subtropical regions of Africa, southern Asia, and northern Australia, mostly in the semi-arid zones. It is commonly found in countries such as Morocco, Algeria, Yemen, Tunisia, Libya, Saudi Arabia, Egypt, India, Iraq, Iran, Pakistan, Bangladesh, Afghanistan, Turkey, Somalia and Sudan.

Cultivation: Henna grows best in latitudes ranging between 15° and 25° N and S from Africa to the Western Pacific. It produces the highest dye content when cultivated in temperatures between 35 °C and 45 °C. The plant grows rapidly by putting out new shoots during the onset of precipitation intervals, after which the growth slows. Gradually, the leaves yellow and fall during prolonged dry or cool intervals. Henna does not thrive below 11 °C and a temperature below 5°C will kill the plant.

Chemical constituents: Carbohydrates, glycosides, tannins, phenolic compounds, gums and mucilage are the main chemical constituents of Henna. It further contains lawsone, apigenin, luteolin, 2-methoxy-3-methyl- 1 ,4-naphthoquinone, cosmosiin and apiin.

Uses: Henna has been found to exhibit antibacterial, antifungal and dermatological properties and is popularly used for coloring skin, scalp and nails. The flowers are intellect promoting and useful in cephalagia, burning sensation, insomnia and fever. The leaves form an extremely important herbal remedy for the management of a diverse spectrum of diseases including wounds, ulcers, cough, bronchitis, lumbago, hemi crania, leucoderma, scabies, boil, hepatopathy, spleenopathy, ophthalmic conditions and jaundice.

Cucumber

Description: Cucumber is a widely cultivated plant in the gourd family Cucurbitaceae, which bears cylindrical edible fruits when ripe. Slicing, pickling and burpless are the three main varieties of cucumber.

Synonym: Cucumis Sativus, Cucumber, kakdi, C. melo and C. citrullus

Geographical origin: Cucumber is originally from India but is now grown on most continents and is believed to be introduced to locations such as Europe by the Greeks and Romans. It is also found in India, France, England and North America.

Cultivation: A few varieties of cucumber are such that the blossoms create seedless fruits without pollination. Pollination for these parthenocarpic varieties degrades the quality. The parthenocarpic varieties are usually grown in greenhouses in the United States, where bees are excluded. In Europe, they are grown outdoors in certain regions where bees are excluded. On the other hand, most cucumber varieties are seeded and require pollination. Therefore thousands of hives of honey bees are annually carried to cucumber fields just before bloom. China, Iran and Turkey are the top producers of cucumber for the year 2010 according to the Food and Agriculture Organization of the United Nations.

Chemical constituents: Phosphorus, potassium, silicon, erepsin, vitamin E, beta-carotene, and folic acid. The fruit of cucumber contains 96.4% moisture, 0.4% protein, 2.8% carbohydrates, 0.01% calcium along with iron, vitamin B and C.

Uses: Cucumber is very useful for skin treatment and natural beautification purposes. It has fat bursting and wrinkle releasing properties. It is extremely effective for treatment of sunburns. Further, cucumber is used to regulate cholesterol levels as well as blood pressure. Even further, it is used for the management of constipation. Cucumber has excellent effects on the skin and even for the eyes. It is called a cool fruit whose effect is believed to bring relief to the eyes in summer. In accordance with another aspect of the present disclosure there is provided a preservative free herbal cosmeceutical composition comprising one or more substances derived from at least one botanical which includes Aloe barbadensis, Rosa sinensis, Emblica officinalis, Eclipta alba, Lawsonia inermis, Curcuma longa and Cucumis sativus and least one excipient. Typically, the preservative free cosmeceutical composition is prepared by the process disclosed in the first aspect of the present disclosure.

The substance used in preparing composition of the present disclosure is derived from various parts of botanicals such as leaves, flowers, fruits, seeds, stem, twigs, branches, bark, stolons, tubers, roots, rhizomes and combinations thereof. Further, the substance is in the form selected from the group that includes but is not limited to extracts, granules, powders, semisolids, isolated fractions, dispersions and oils. In one embodiment, the substance is in the form of an extract. Typically, the extract is selected from the group that include but are not limited to alcoholic, hydro-alcoholic and aqueous extract. Further, the extract is prepared by using techniques selected from the group that includes but is not limited to Soxhlet extraction, percolation, decoction, maceration and supercritical fluid extraction.

Typically, the excipient includes surfactants, emulsifiers, vehicles, gelling agents, oils, waxes, emollients, perfumes, coloring agents, propellants, opacifiers, humectants, antioxidants, suspending agents, penetration enhancers, thickening agents, antifoaming agents, scrub beads and plasticizers.

The surfactant used in preparing the composition of the present disclosure is at least one selected from the group that includes but is not limited to triethanolamine, alkyl polyethylene oxide, alkylphenol polyethylene oxide, sodium laureth sulphate, sodium dodecyl sulphate, alkyl alcohol, sodium lauryl sulfate, polyoxyethylene/polyoxypropylene block polymers (poloxamers), glycerols, polyglycerols, fatty acids, polyethylene glycol hydroxy stearate, polyalkyl glucosides, ceramides, polyethylene glycol/alkyl glycol copolymers, and polyethylene glycol/polyalkylene glycol ether di-block or tri-block copolymers, diacetylated monoglycerides, diethylene glycol monostearate, ethylene glycol monostearate, glyceryl monooleate, propylene glycol monostearate, macrogol esters, macrogol stearate, polyoxyethylene 50 stearate, macrogol ethers, cetomacrogol 1000, lauromacrogols, nonoxynols, octoxinols, tyloxapol, polyvinyl alcohols, polysorbate, sorbitan monolaurate, sorbitan monooleate, sorbitan monopalmitate, sorbitan sesquioleate, sorbitan trioleate, sorbitan tristearate, sucrose esters, cetyl alcohol, oleyl alcohol, cetylpyridinium chloride, cetyl trimethylammonium bromide, tween 20 and tween 80.

Typically, the oil is at least one selected from the group that includes but is not limited to isopropyl myristate, myristyl myristate, isopropyl palmitate, isopropyl stearate, isopropyl oleate, n-butyl stearate, n-hexyl laurate, n-decyl oleate, isooctyl stearate, isononyl stearate, isononyl isononanoate, 2-ethylhexyl palmitate, 2-ethylhexyl laurate, 2-hexyldecyl stearate, 2- octyldodecyl palmitate, oleyl oleate, ethylhexyl cocoate, dicaprylyl carbonate, cetearyl isononanoate, oleyl erucate, erucyl oleate, erucyl erucate, octyldodecanol, polydecenes, squalane, dicaprylyl ether, butylene glycol dicaprylate/dicaprate, caprylic/capric triglyceride, olive oil, sunflower oil, soybean oil, peanut oil, rapeseed oil, almond oil, palm oil, coconut oil, palm kernel oil, castor oil, wheat germ oil, grape seed oil, thistle oil, silicon oils, lanolin oil, avocado oil and macadamia oil.

The wax used in the preparing composition of the present disclosure is at least one selected from the group that includes but is not limited to candelilla wax, carnauba wax, bees wax, esparto grass wax, cork wax, guaruma wax, rice germ oil wax, sugarcane wax, berry wax, ouricury wax, montan wax, jojoba wax, shea butter, beeswax, shellac wax, spermaceti, lanolin (wool wax), uropygial grease, ceresin, ozocerite (earth wax), paraffin waxes, sunflower wax, lemon wax, grape fruit wax and laurel wax.

Typically, the thickening agent is at least one selected from the group that includes but is not limited to hydroxypropyl methylcellulose, hydroxypropyl cellulose, sodium carboxy methyl cellulose, hydroxyethyl cellulose, carbopol polyethylene glycol, acrylates, methacrylates, gelatin, alginates, pectins, tragacanth, karaya gum, xanthan gum, carrageenin, agar, alginate, chitosan and acacia.

Typically, the emollient is at least one selected from the group that includes but is not limited to stearic acid, caprylic acid, oleic acid, palmitic acid, lauric acid, cetyl alcohol, lauryl alcohol, stearyl alcohol, cetearyl alcohol, oleyl alcohol, octyl palmitate, octyl stearate, glyceryl stearate, propylene glycol, dicaprate, dicaprylate and cetyl palmitate.

Typically, the humectant is at least one selected from the group that includes but is not limited to glycerin, sorbitol, propylene glycol, hexylene glycol, butylene glycol, MP Diol, Urea & alpha-hydroxy acids (AHA's), sodium-2-pyrrolidone-5- carboxylate (Sodium PCA), glucose, fructose, proteins, amino acids, short chain ethers, vitamins, erythritol, capryl glycol and phytantriol.

Typically, the antifoaming agent is at least one selected from the group that includes but is not limited to silicone emulsion, polyethylene oxide-poly propylene oxide (peo-ppo) block copolymer, phenethyl disiloxane, tetramethyl decynediol, polysilicone-7, phenyl trimethicone, bisphenyl-hexamethicone, simethicone, dimethicone, dimethiconol, hexamethyl-disiloxane, silica dimethyl silylate, silica silylate, hexyl alcohol, isopropyl alcohol, octyl alcohol, propyl alcohol and petroleum distillates.

Typically, the perfume is at least one selected from the group that includes but is not limited to citrus musk, floral woody, citrus musk woody, fresh bouquet, musk, floral musk, lavender oil, jasmine oil, rose oil, cedarwood oil, sandalwood oil, orange oil and lemon oil.

In one embodiment, the composition includes at least one excipient selected from the group comprising carbomer, polyethylene glycol, CAPB, polysorbate 20, disodium EDTA, sodium hydroxide and glycerin.

In accordance with yet another aspect of the present disclosure there is provided a pack containing preservative free herbal cosmeceutical of the present disclosure.

Typically the pack is selected from the group consisting of heat sealable pouch, tubes, sachets, pouches, vials, bottles, cans, tubes and tins.

The present disclosure is further described in the light of the following examples which are set forth for illustration purpose only and not to be construed for limiting the scope of the disclosure.

Example 1:

For preparing a preservative free herbal skin moisturizer, 3 gm of carbomer was dispersed in demineralized water to obtain a dispersion. 60 gm of Aloe vera extract, 0.5 mg of disodium EDTA and 0.5 mg of sodium hydroxide was mixed in the dispersion to obtain a gel. The quantities of each of the ingredients were as per Table 1.

The gel was then filled and subsequently sealed in pre-sterilized heat sealable pouches aseptically. The sealed pouches were then autoclaved at a temperature of 121°C, for a time period of 30 minutes to obtain a preservative free herbal cosmeceutical composition in the form of gel.

Table 1:

Example 2:

For preparing a preservative free herbal composition to control hair fall, the procedure described in example lwas repeated by using the ingredients as given in Table 2.

Table 2

7 Disodium EDTA 1.5 gm

8 Sodium hydroxide 0.5mg

9 Aroma q.s.

10 Demineralized water q.s.

Example 3:

For preparing a preservative free herbal skin cleansing gel, the procedure described in example l as repeated by using the ingredients as given in Table 3.

Table 3:

Example 4:

For preparing a preservative free herbal skin toner, the procedure described in example 1 was repeated by using the ingredients as given in Table 4.

Table 4:

Example 5:

For preparing a preservative free herbal hair conditioner, the procedure described in example lwas repeated by using the ingredients as given in Table 5.

Table 5:

6 Aroma q.s.

7 Demineralized water q.s.

Throughout this specification the word "comprise", or variations such as "comprises" or "comprising", will be understood to imply the inclusion of a stated element, integer or step, or group of elements, integers or steps, but not the exclusion of any other element, integer or step, or group of elements, integers or steps.

The use of the expression "a", "at least" or "at least one" suggests the use of one or more elements or ingredients or quantities, as the use may be in the embodiment of the disclosure to achieve one or more of the desired objects or results.

The numerical values given for various physical parameters, dimensions and quantities are only approximate values and it is envisaged that the values higher or lower than the numerical value assigned to the physical parameters, dimensions and quantities fall within the scope of the disclosure and the claims unless there is a statement in the specification to the contrary.

While certain embodiments of the disclosure have been described, these embodiments have been presented by way of examples only, and are not intended to limit the scope of the disclosure. Variations or modifications in the process of this disclosure, within the scope of the disclosure, may occur to those skilled in the art upon reviewing the disclosure herein. Such variations or modifications are well within the spirit of this disclosure.