Title:
METHOD AND APPARATUS FOR PRODUCING SATURATED CARBOXYLIC ACID HAVING 1-4 CARBON ATOMS
Document Type and Number:
Japanese Patent JP3542757
Kind Code:
B2
Abstract:
PROBLEM TO BE SOLVED: To provide a method and apparatus for producing a 1-4C saturated carboxylic acid, capable of obtaining a high acid yield and producing a by- product as an high-value-added substance.
SOLUTION: When a reaction outlet gas is partially returned during reaction gas circulation and acid concentration in content returned by a separation process is decreased, a saturated or unsaturated 4C hydrocarbon or a mixture thereof is subjected to vapor phase oxidation in the presence of an oxygen- containing gas and steam at temperature of 100-400°C reaction temperature under a pressure of 1.2×105 Pa to 51×05 Pa by using at least one catalyst to produce a 1-4C saturated carboxylic acid. In the production method, a crude acid is separated from reaction outlet gas by counterflow cleaning. Thereby, high selectivity is obtained and necessary energy consumption is decreased and high passive safety against danger of explosion is obtained and whole process execution can simply be formed thereby.
Inventors:
Christoph Rüdinger
Hans-Jürgen Eberle
Michael Harman
Hans-Jürgen Eberle
Michael Harman
Application Number:
JP2000063970A
Publication Date:
July 14, 2004
Filing Date:
March 08, 2000
Export Citation:
Assignee:
Consortium fuer elektrochemische Industrie GmbH
International Classes:
B01J23/28; C07B61/00; C07C51/21; C07C51/215; C07C51/25; C07C51/42; C07C51/48; B01J23/22; C07C53/02; C07C53/08; C07C53/122; (IPC1-7): C07C51/25; B01J23/22; B01J23/28; C07B61/00; C07C51/215; C07C53/08; C07C53/122
Domestic Patent References:
JP2000026363A | ||||
JP2000026364A | ||||
JP2000505723A | ||||
JP2001523237A | ||||
JP50017969B1 |
Attorney, Agent or Firm:
Toshio Yano
Toshiomi Yamazaki
Takuya Kuno
Einzel Felix-Reinhard
Reinhard Einsel
Toshiomi Yamazaki
Takuya Kuno
Einzel Felix-Reinhard
Reinhard Einsel
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