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Patent Searching and Data


Title:
METHOD OF MANUFACTURING CARBON NANOTUBE
Document Type and Number:
Japanese Patent JP2005001938
Kind Code:
A
Abstract:

To provide a method of manufacturing a carbon nanotube (CNT) by which the production quantity of the carbon nanotube is changed without changing the synthetic condition such as a synthetic time and a flow rate of a gaseous starting material.

A substrate 1 composed of an alloy (Cu-Ni alloy) of Ni which is a CNT forming catalyst and Cu which is a non-forming catalyst is set in a reaction tube 2. A synthetic part 8 is heated to 700°C by an infrared image furnace 4. Acetylene is supplied at a flow rate of 100 cm3/min from a pipe 7a, argon is supplied at a flow rate of 20 cm3/min from a pipe 7b and an exhausted gas is discharged from a pipe 7c. The state is kept for 10 min to react the catalytic metal with acetylene. At this time, the temperature of the substrate 1 is measured by a thermocouple 3 and the temperature of the infrared image furnace 4 is controlled based on the temperature of the substrate 1 by a temperature controller 5 to keep the temperature of the synthetic part 8 at 700°C. As a result, the CNT is formed in the quantity corresponding to Ni content in the substrate 1 on the substrate 1.


Inventors:
KATAYAMA SHINJI
TANABE NOBUO
USUI HIROKI
Application Number:
JP2003166872A
Publication Date:
January 06, 2005
Filing Date:
June 11, 2003
Export Citation:
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Assignee:
FUJIKURA LTD
International Classes:
C01B31/02; B01J23/755; C23C16/26; (IPC1-7): C01B31/02; B01J23/755; C23C16/26
Attorney, Agent or Firm:
Masanori Fujimaki