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Title:
PROCESS FOR PRODUCING HYDROXYALKYL (METH)ACRYLATE
Document Type and Number:
Japanese Patent JP2014031326
Kind Code:
A
Abstract:

To provide a process for producing hydroxyalkyl (meth)acrylate efficiently by recovering a catalyst maintaining a sufficient activity from a distillation apparatus and reusing it.

Provided is a process for producing a hydroxyalkyl (meth)acrylate comprising the steps of: reacting (meth)acrylic acid with an alkylene oxide in the presence of a catalyst; and purifying a hydroxyalkyl (meth)acrylate by distillation from a reaction mixture obtained by the reaction. In the distillation purification step, n (n represents an integer equal to 2 or more) stage distillation is performed using n distillation apparatuses; and at least a portion of residual liquid obtained in a (n-1)th or earlier stage is used in a reaction step conducted separately from the above reaction step.


Inventors:
ISHIDA NORIMASA
TAKAGI HIROYUKI
NAKAMURA MASATAKA
JINNO HIROSHI
Application Number:
JP2012172278A
Publication Date:
February 20, 2014
Filing Date:
August 02, 2012
Export Citation:
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Assignee:
NIPPON CATALYTIC CHEM IND
International Classes:
C07C67/26; C07C67/54; C07C69/54; C07B61/00
Domestic Patent References:
JP2008127302A2008-06-05
JP2008074795A2008-04-03
JP2012012348A2012-01-19
JP2001106654A2001-04-17
Foreign References:
WO2006013971A12006-02-09
WO2008133222A12008-11-06
Attorney, Agent or Firm:
Kyuichi Ueki
Hisahiko Ueki
Tadashi Sugakawa
Hiroaki Ito