Title:
Mass spectrometry method, chromatograph mass spectrometer, and mass spectrometry program
Document Type and Number:
Japanese Patent JP6288313
Kind Code:
B2
Abstract:
A mass spectrometry method includes: creating a plurality of measurement conditions corresponding to all combinations of precursor-ion candidates generated from the target compound and collision-energy-value candidates; performing a product-ion scan measurement using each of the plurality of measurement conditions and performing a plurality of reference measurements for detecting a predetermined kind of ion generated from the target compound under the same condition, within an introduction time during which the target compound is introduced; creating a peak function, which is a function representing a change in the amount of introduction of the target compound into the mass spectrometer within the introduction time, based on the result of the reference measurement; creating a normalization function for normalizing the amount of introduction of the target compound within the introduction time, based on the peak function; and normalizing the intensity of product-ion spectra obtained by the product-ion scan measurements performed for all combinations.
Inventors:
Takashi Sumiyoshi
Application Number:
JP2016572996A
Publication Date:
March 07, 2018
Filing Date:
February 04, 2015
Export Citation:
Assignee:
SHIMADZU CORPORATION
International Classes:
G01N27/62
Domestic Patent References:
| JP2013234859A | ||||
| JP2013015485A | ||||
| JP2010054406A |
Foreign References:
| US20120158318 |
Other References:
滝埜 昌彦,「液体クロマトグラフィー/質量分析法の農薬残留分析への利用(その2) -LC-MS/MSおよびLC-Q/TOFMSを用いた,日本農薬学会誌,2012年 8月20日,Vol. 37, No. 3,pp. 297-302
伊達 英代, 他4名,「健康食品中に含まれる経口血糖降下薬の系統的分析法」,薬学雜誌,社団法人日本薬学会,2009年 1月 1日,Vol. 129, No.1,pp. 163-172
伊達 英代, 他4名,「健康食品中に含まれる経口血糖降下薬の系統的分析法」,薬学雜誌,社団法人日本薬学会,2009年 1月 1日,Vol. 129, No.1,pp. 163-172
Attorney, Agent or Firm:
Kyoto International Patent Office
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