Title:
CARBON NANOCOIL-CARBON MICROCOIL HYBRID MATERIAL, AND PREPARATION METHOD THEREFOR
Document Type and Number:
WIPO Patent Application WO/2017/175906
Kind Code:
A1
Abstract:
The present invention relates to a carbon nanocoil-carbon microcoil hybrid material, and a preparation method therefor, the method comprising the steps of: arranging a ceramic substrate within a deposition chamber for carrying out thermal chemical vapor deposition; and injecting, into the deposition chamber, C2H2 gas as a raw material gas and SF6 gas as an additional gas, wherein the C2H2 gas is injected during the entire deposition time and the SF6 gas is injected by modulating between ON-OFF at least twice, thereby enabling the preparation of a carbon nanocoil-carbon microcoil hybrid material synthesized by artificially controlling the injection of SF6 gas according to reaction time.
Inventors:
KIM SUNG HOON (KR)
KANG GI HWAN (KR)
PARK SANG MOON (KR)
KANG GI HWAN (KR)
PARK SANG MOON (KR)
Application Number:
PCT/KR2016/004066
Publication Date:
October 12, 2017
Filing Date:
April 19, 2016
Export Citation:
Assignee:
UNIV SILLA (KR)
International Classes:
B81B1/00; B82B1/00; C23C16/26
Foreign References:
| KR20140028318A | 2014-03-10 |
Other References:
YANG, SHAOMING ET AL.: "Morphology and Microstructure of Spring-like Carbon Micro-coils/nano-coils Prepared by Catalytic Pyrolysis of Acetylene Using Fe-containing Alloy Catalysts", CARBON, vol. 43, 2005, pages 827 - 834, XP027645176
EUM, JUN-HO ET AL.: "Effect of Gas Phase Composition Cycling on/off Modulation Numbers of C2H2/SF6 Flows on the Formation of Geometrically Controlled Carbon Coils", JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, vol. 12, no. 7, 2012, pages 6100 - 6106
EUM, JUN-HO ET AL.: "Large-scale Synthesis of the Controlled-geometry Carbon Coils by the Manipulation of the SF6 Gas Flow Injection Time", JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, vol. 12, no. 5, 2012, pages 4397 - 4402, XP055430956
JEON, YOUNG-CHUL ET AL.: "Large-scale Synthesis of the Carbon Coils Using Stainless Steel Substrate", JOURNAL OF THE KOREAN CRYSTAL GROWTH AND CRYSTAL TECHNOLOGY, vol. 23, no. 6, 2013, pages 296 - 301, XP055430961
HIKITA, MUNEAKI ET AL.: "Growth and Properties of Carbon Microcoils and Nanocoils", CRYSTALS, vol. 4, 2014, pages 466 - 489, XP055430964
EUM, JUN-HO ET AL.: "Effect of Gas Phase Composition Cycling on/off Modulation Numbers of C2H2/SF6 Flows on the Formation of Geometrically Controlled Carbon Coils", JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, vol. 12, no. 7, 2012, pages 6100 - 6106
EUM, JUN-HO ET AL.: "Large-scale Synthesis of the Controlled-geometry Carbon Coils by the Manipulation of the SF6 Gas Flow Injection Time", JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, vol. 12, no. 5, 2012, pages 4397 - 4402, XP055430956
JEON, YOUNG-CHUL ET AL.: "Large-scale Synthesis of the Carbon Coils Using Stainless Steel Substrate", JOURNAL OF THE KOREAN CRYSTAL GROWTH AND CRYSTAL TECHNOLOGY, vol. 23, no. 6, 2013, pages 296 - 301, XP055430961
HIKITA, MUNEAKI ET AL.: "Growth and Properties of Carbon Microcoils and Nanocoils", CRYSTALS, vol. 4, 2014, pages 466 - 489, XP055430964
Attorney, Agent or Firm:
LEE, Han-Ook (KR)
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