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Title:
PROCESS FOR OBTAINING COMPOUND TROUGH PRECIPITATION OF SILICA INTO LATEX
Document Type and Number:
WIPO Patent Application WO/2014/024124
Kind Code:
A4
Abstract:
Although the addition of precipitated silica confers peculiar mechanical properties to rubber compounds enabling its application in several areas, Its incorporation process is extremely complex due to the difficult dispersion of silica in the elastomeric matrix, equipment wear and risk to the operators. The silica sequential precipitation process from any alkali silicate in an emulsion of latex of any origin not only enables the homogeneous distribution of silica in the elastomeric matrix, but also decreases the costs from the reduced wear of the rubber processing equipment and reduced production time, since the silica is already homogeneously incorporated into the matrix.

Inventors:
PILECCO ONÉLIO (BR)
PIEROZAN NILSO JOSÉ (BR)
MOTA MARTON LUIZ FERNANDO (BR)
Application Number:
PCT/IB2013/056415
Publication Date:
September 12, 2014
Filing Date:
August 05, 2013
Export Citation:
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Assignee:
PILECCO ONÉLIO (BR)
PANCIERA PILECCO FÁBIO (BR)
PILECCO SONEGO ROSANE TEREZINHA (BR)
International Classes:
C08J3/26
Attorney, Agent or Firm:
SUL AMERICA MARCAS E PATENTES LTDA (LeonorRua Luis Gois, 129, -150 São Paulo SP, BR)
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Claims:
AMENDED CLAIMS

received by the International Bureau on 1 1 March 2014 (1 1.03.2014).

1. A process, and the product resulted therein, of silica-added rubber compounds / composites, at any content in the range from 5 to 200 prh, wet route, where a composition containing latex, alkaline silicate and additives, appropriately stabilized is fed simultaneously with acid in the reactor ("in situ" precipitation), under well defined pH (typically 9), temperature (typically 85°C) , time {typically 70 minutes) and vigorous stirring conditions, characterized by the fact that the precipitation of the silica occurs first with morphological properties controlled by these conditions and later coagulation of the resulting latex composition, where the silica becomes homogeneously distributed and totally incorporated in the rubber clots / lumps and whose prepared compounds present extremely elevated physical-chemical properties.