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Title:
脂肪酸の自己触媒エステル化のための方法
Document Type and Number:
Japanese Patent JP5808479
Kind Code:
B2
Abstract:
The present invention relates to a process for isolation of micronutrients from deodorizer distillate comprising free fatty acids, the process comprises the following steps: (i) treating the deodorizer distillate in an esterification step with glycerol, which esterification step is autocatalyzed, producing a feedstock of acyl glycerides, and discharging excess of glycerol and produced water; (ii) transferring the feedstock of acyl glycerides having a water content less than 1500 ppm and a free fatty acid content less than 3 wt % to a transesterification step and treating the feedstock of acyl glycerides with methanol to produce a crude biodiesel product; and (iii) refining the crude biodiesel product in a distillation step, and separating the crude biodiesel product into three fractions 1) fatty acid methyl esters, 2) micronutrient rich product comprising tocopherol, and 3) light hydrocarbons.

Inventors:
Suzanne Johnson
Bent Sarp
Application Number:
JP2014504311A
Publication Date:
November 10, 2015
Filing Date:
April 12, 2012
Export Citation:
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Assignee:
Alpha-Laval Corporate Arb
International Classes:
C11C3/10; C10L1/02; C11C3/06
Domestic Patent References:
JP8500598A
JP57016878A
JP2007502271A
Attorney, Agent or Firm:
Yasuhiko Murayama
Masatake Shiga
Takashi Watanabe
Shinya Mitsuhiro