Title:
自動試験プロトコル
Document Type and Number:
Japanese Patent JP2004515770
Kind Code:
A
Abstract:
A method and apparatus for automating the qualification process for chromatographic systems. Automation technology and regression analysis are used for qualifying a chromatography system. The trained operator prepares the chromatography system to ensure that the samples, solvents, and the separation column are ready for analysis. The qualification of the detector, the solvent delivery system, the sample manager, the gradient proportioning system, the column heater, and the delay volume of the chromatography system are completed without the necessity of operator intervention. Regression analysis is performed to compute performance statistics that demonstrate the accuracy, linearity, and precision of the chromatographic system and quantify its suitability for chromatographic analysis.
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| JPH0718851 | Description: High Performance Liquid Chromatograph |
Inventors:
Andrews, Richard Wayne
Corbin, Virginia El
Corbin, Virginia El
Application Number:
JP2002548658A
Publication Date:
May 27, 2004
Filing Date:
December 05, 2001
Export Citation:
Assignee:
Waters Investments Limited
International Classes:
G01N30/02; G01N30/34; G01N30/54; G01N30/74; G01N30/86; G01N30/88; (IPC1-7): G01N30/02; G01N30/34; G01N30/54; G01N30/74; G01N30/86
Domestic Patent References:
| JPH03269258A | 1991-11-29 | |||
| JPH09274028A | 1997-10-21 | |||
| JPH05322870A | 1993-12-07 | |||
| JPH09171022A | 1997-06-30 | |||
| JP2000136999A | 2000-05-16 | |||
| JPH07120451A | 1995-05-12 | |||
| JPH01174965A | 1989-07-11 | |||
| JP2000275253A | 2000-10-06 |
Other References:
松下 至: "ＨＰＬＣ装置導入時に必要な技術と知識", ケミアル・エンジニヤリング, vol. 45, no. 6, JPN6007012430, 1 June 2000 (2000-06-01), pages 464 - 466, ISSN: 0000942175
斉藤 紘史: "計量管理 −測定法の評価のためのＳＮ比の利用について", 工業用水, vol. 315, no. 12, JPN6007012432, 20 December 1984 (1984-12-20), pages 25 - 32, ISSN: 0000942176
WANG Q., GAO R., YAN B.,AND FAN D.: "Computer-assisted Optimization of Grandient Elution High-performance Liquid Chromatography", FENXI HUAXUE, vol. 22, no. 5, JPN4006016029, 20 May 1994 (1994-05-20), CN, pages 495 - 498, ISSN: 0000767168
SCHOENMAKERS P.J., DUNAND N.: "Explanations and advice provided by an expert system optimization in high-performance liquid chromat", JOURNAL OF CHROMATOGRAPHY, vol. 485, JPN4006016030, 27 December 1989 (1989-12-27), pages 219 - 236, XP026550702, ISSN: 0000767169, DOI: 10.1016/S0021-9673(01)89140-8
斉藤 紘史: "計量管理 −測定法の評価のためのＳＮ比の利用について", 工業用水, vol. 315, no. 12, JPN6007012432, 20 December 1984 (1984-12-20), pages 25 - 32, ISSN: 0000942176
WANG Q., GAO R., YAN B.,AND FAN D.: "Computer-assisted Optimization of Grandient Elution High-performance Liquid Chromatography", FENXI HUAXUE, vol. 22, no. 5, JPN4006016029, 20 May 1994 (1994-05-20), CN, pages 495 - 498, ISSN: 0000767168
SCHOENMAKERS P.J., DUNAND N.: "Explanations and advice provided by an expert system optimization in high-performance liquid chromat", JOURNAL OF CHROMATOGRAPHY, vol. 485, JPN4006016030, 27 December 1989 (1989-12-27), pages 219 - 236, XP026550702, ISSN: 0000767169, DOI: 10.1016/S0021-9673(01)89140-8
Attorney, Agent or Firm:
Kazuo Shamoto
Tadashi Masui
Yasushi Kobayashi
Akio Chiba
Hiroyuki Tomita
Hideo Tanaka
Tadashi Masui
Yasushi Kobayashi
Akio Chiba
Hiroyuki Tomita
Hideo Tanaka