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Patent Searching and Data


Title:
BETA-CHLORO ACRYLALDEHYDE DERIVATIVE, ITS PRODUCTION, ITS USE AND ITS PRODUCTION INTERMEDIATE
Document Type and Number:
Japanese Patent JPH10139710
Kind Code:
A
Abstract:

To obtain a new compound useful as an intermediate for producing a compound having insecticidal activity industrially advantageously in terms of safety, operability and economy.

This compound is shown by formula I (X is H or F; R is a 1-8C alkyl or a 1-2C alkyl which is substituted with one or more fluorine atoms)) such as 3-chloro-4-(4-ethoxyphenyl)-7-(4-fluoro-3-phenoxyphenyl)-3-methyl-2- heptenol. The compound of formula I is obtained by reacting (A) a compound of formula II with a compound of formula III in a solvent in the presence of a phase transfer catalyst and an alkali metal hydroxide to give a carbonyl compound of formula IV, treating the compound with (B) a chlorine compound selected from phosphorus oxychloride, carbonyl chloride, oxalyl chloride and phosphorus pentoxide and (C) an amide compound which is N-dimethylformamide or N-methylformanilide and hydrolyzing the resulting substance.


Inventors:
TAKAGAKI TOHEI
OTSUKA SUSUMU
MATSUO NORITADA
TSUSHIMA KAZUHIRO
Application Number:
JP29884196A
Publication Date:
May 26, 1998
Filing Date:
November 11, 1996
Export Citation:
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Assignee:
SUMITOMO CHEMICAL CO
International Classes:
C07C41/18; C07B61/00; C07C43/285; C07C43/29; C07C45/42; C07C45/67; C07C45/68; C07C47/277; C07C49/255; (IPC1-7): C07C47/277; C07C41/18; C07C43/285; C07C43/29; C07C45/42; C07C45/67; C07C49/255
Attorney, Agent or Firm:
Takashi Kuboyama (1 person outside)