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Title:
METHOD FOR PRODUCING dl-1,2-DIPHENYLETHYLENEDIAMINE
Document Type and Number:
Japanese Patent JP2006124325
Kind Code:
A
Abstract:

To provide a method for producing dl-1,2-diphenylethylenediamine, capable of efficiently synthesizing the product through simple processes, by decreasing a number of the processes and improving reaction conditions.

This method includes a process for reacting hydrobenzamide with an organic base in an aprotic polar solvent, a process for adding acetic anhydride to the reaction mixture and acetylating the mixture in the presence of an acetate salt, and a process for adding water to the acetylated reaction mixture, further adding acetic acid and an inorganic acid thereto, and hydrolyzing the mixture.


Inventors:
FUJIMOTO KENJI
Application Number:
JP2004314714A
Publication Date:
May 18, 2006
Filing Date:
October 28, 2004
Export Citation:
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Assignee:
FUJI MOLECULAR PLANNING CO LTD
International Classes:
C07C209/62; C07C211/27; C07B53/00
Domestic Patent References:
JP2000086593A2000-03-28
JPH1112232A1999-01-19
JP2000086593A2000-03-28
JPH1112232A1999-01-19
Other References:
JPN4007017056, WEI−PING, C. and FU−QIU, Y., Chinese Journal of Pharmaceuticals, 1993, 24(6), p.280−281
Attorney, Agent or Firm:
Kato Asamichi