Title:
METHOD FOR EFFICIENTLY PRODUCING BIS(TRIFLUOROACETYL) PEROXIDE
Document Type and Number:
Japanese Patent JP3448649
Kind Code:
B2
Abstract:
PROBLEM TO BE SOLVED: To provide an industrially excellent method for readily producing bis(trifluoroacetyl)peroxide by which the bis(trifluoroacetyl)peroxide can be produced in a short time in high yield.
SOLUTION: This method for readily producing the bis(trifluoroacetyl) peroxide is characterized in that trifluoroacetic anhydride is reacted with sodium peroxide dispersed in acetonitrile. Preferably, the initial molar ratio of the trifluoroacetic anhydride to the sodium peroxide is regulated within the range of 2.0-2.5 in the method.
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| WO/1995/030653 | PROCESS FOR PERACID MANUFACTURE |
Inventors:
Yoshio Hayakawa
Naohiro Terasawa
Naohiro Terasawa
Application Number:
JP2000378296A
Publication Date:
September 22, 2003
Filing Date:
December 13, 2000
Export Citation:
Assignee:
National Institute of Advanced Industrial Science and Technology
International Classes:
C07C407/00; C07C409/36; (IPC1-7): C07C407/00; C07C409/36
Domestic Patent References:
| JP1249752A |
Other References:
Ｊｏｕｒｎａｌ ｏｆ Ｆｌｕｏｒｉｎｅ Ｃｈｅｍｉｓｔｒｙ，１９９０，Ｖｏｌ．４６，Ｐ４２３−４３１