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Title:
METHOD FOR PRODUCING CARBOXYLIC CHLORIDE FOR COLOR COUPLER INTERMEDIATE
Document Type and Number:
Japanese Patent JP2003026630
Kind Code:
A
Abstract:

To provide a method for industrially and easily producing high-purity carboxylic acid chlorides for color coupler intermediates having good hue and not containing a sulfur component giving bad influences on a photographic performance.

This method for producing carboxylic acid chlorides for color coupler intermediates comprises reacting 1 mol monovalent carboxylic acid with 0.5-1.0 mol phosphorus oxychloride in the presence of 0.2-1.5 mol N,N- dimethylformamide in ≤10C aromatic solvent and then removing the by-product by a liquid phase separation.


Inventors:
KATSUMURA YASUO
NAKA YOSHIMASA
KADOTA YOSHIKO
ISSHIKI TSUNEKI
Application Number:
JP2001212928A
Publication Date:
January 29, 2003
Filing Date:
July 13, 2001
Export Citation:
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Assignee:
TAOKA CHEMICAL CO LTD
International Classes:
C07C51/60; C07B61/00; C07C53/42; C07C59/68; (IPC1-7): C07C51/60; C07C53/42; C07C59/68
Domestic Patent References:
JPS3817009B1
JPS4310613B1
JPS5959643A1984-04-05
JPH04224542A1992-08-13
JPH05339194A1993-12-21
JPH09110782A1997-04-28
JPS5427532A1979-03-01
JPH06279380A1994-10-04