Title:
METHOD FOR PRODUCING CARBOXYLIC CHLORIDE FOR COLOR COUPLER INTERMEDIATE
Document Type and Number:
Japanese Patent JP2003026630
Kind Code:
A
Abstract:
To provide a method for industrially and easily producing high-purity carboxylic acid chlorides for color coupler intermediates having good hue and not containing a sulfur component giving bad influences on a photographic performance.
This method for producing carboxylic acid chlorides for color coupler intermediates comprises reacting 1 mol monovalent carboxylic acid with 0.5-1.0 mol phosphorus oxychloride in the presence of 0.2-1.5 mol N,N- dimethylformamide in ≤10C aromatic solvent and then removing the by-product by a liquid phase separation.
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Inventors:
KATSUMURA YASUO
NAKA YOSHIMASA
KADOTA YOSHIKO
ISSHIKI TSUNEKI
NAKA YOSHIMASA
KADOTA YOSHIKO
ISSHIKI TSUNEKI
Application Number:
JP2001212928A
Publication Date:
January 29, 2003
Filing Date:
July 13, 2001
Export Citation:
Assignee:
TAOKA CHEMICAL CO LTD
International Classes:
C07C51/60; C07B61/00; C07C53/42; C07C59/68; (IPC1-7): C07C51/60; C07C53/42; C07C59/68
Domestic Patent References:
JPS3817009B1 | ||||
JPS4310613B1 | ||||
JPS5959643A | 1984-04-05 | |||
JPH04224542A | 1992-08-13 | |||
JPH05339194A | 1993-12-21 | |||
JPH09110782A | 1997-04-28 | |||
JPS5427532A | 1979-03-01 | |||
JPH06279380A | 1994-10-04 |
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