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Title:
METHOD FOR PRODUCING EPOXY COMPOUND
Document Type and Number:
Japanese Patent JP2016034913
Kind Code:
A
Abstract:
PROBLEM TO BE SOLVED: To provide a method for producing an epoxy compound which enables reuse of a catalyst while using a tungsten peroxide compound as a catalyst, and can be preferably applied to an industrial production process.SOLUTION: A method for producing an epoxy compound includes: an epoxidization step of obtaining a reaction mixture containing an epoxy compound by an epoxidization reaction of an olefin compound which uses a tungsten peroxide compound as a catalyst and hydrogen peroxide as an oxidant; a solvent removable step of removing a solvent from the reaction mixture through atmospheric distillation or reduced-pressure distillation; an extraction step of adding an extraction solvent to the reaction mixture through the solvent removable step, and obtaining an extract containing the epoxy compound and the extraction solvent and an extraction residue containing the catalyst; a separation step of separating the epoxy compound from the extract through the distillation; and a reuse step of reusing in the epoxidization step, the catalyst contained in the extraction residue.SELECTED DRAWING: Figure 1

Inventors:
OKAZAKI MOTOYA
SEGAWA ATSUSHI
MATSUMOTO TAKANARI
MIZUNO TETSUTAKA
KAMATA KEIGO
Application Number:
JP2014157823A
Publication Date:
March 17, 2016
Filing Date:
August 01, 2014
Export Citation:
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Assignee:
UNIV TOKYO
JX NIPPON OIL & ENERGY CORP
International Classes:
C07D303/04; C07D301/12
Domestic Patent References:
JP2013241376A2013-12-05
JP2013184850A2013-09-19
JPS59108793A1984-06-23
Foreign References:
WO2014175152A12014-10-30
WO2013133009A12013-09-12
Attorney, Agent or Firm:
Yoshiki Hasegawa
Yoshiki Kuroki
Yoshinori Shimizu
Hiroyuki Hirano