Title:
PHOTOCHLORINATION OF PHTHALIC ANHYDRIDE
Document Type and Number:
Japanese Patent JP3252920
Kind Code:
B2
Abstract:
PURPOSE: To obtain 4-chlorophthalic acid anhydride with high yield by irradiating phthalic acid anhydride and chlorine with light.
CONSTITUTION: Chlorine and phthalic acid anhydride in a vapor phase are sent to a reaction chamber and irradiated with light (preferably UV rays) to obtain chlorinated phthalic acid anhydride having at least 5:1 ratio of (4 chlorophthalic acid anhydride):(3-chlorophthalic acid anhydride). The reaction is preferably carried out at 275 to 325°C and the ratio of (chlorine):(phthalic acid anhydride) is preferably 1:1 to 2:1.
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Inventors:
Carl W. Separ
John Earl Molinaro
John Earl Molinaro
Application Number:
JP9971292A
Publication Date:
February 04, 2002
Filing Date:
April 20, 1992
Export Citation:
Assignee:
Occidental Chemical Corporation
International Classes:
C07D307/89; C07B39/00; C07C51/567; (IPC1-7): C07D307/89; C07B39/00
Domestic Patent References:
JP5088074A | ||||
JP63130559A |
Other References:
J.Org.Chem.,48(15),p.2465−2468(1983)
Attorney, Agent or Firm:
Minoru Nakamura (6 outside)
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