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Title:
PRODUCTION OF 1-AMINO-2-BROMO-4-HYDROXYANTHRAQUINONE
Document Type and Number:
Japanese Patent JPH10130213
Kind Code:
A
Abstract:

To provide a profitable method for producing 1-amino-2-bromo-4- hydroxyanthraquinone, excellent in operability and washing efficiency, and not causing a problem related to the corrosion of a drying machine and a product-filling machine after the washing operation.

This method for producing 1-amino-2-bromo-4- hydroxyanthraquinone comprises dibrominating 1-aminoanthraquinone in concentrated sulfuric acid under heating, hydrolyzing the obtained 1-amino-2,4- dibromoanthraquinone in the presence of a boric acid in the sulfuric acid, in necessary, increased in the concentration without isolating the product, and subsequently neutralizing the deposited 1-amino-2-bromo-4-hydroxyanthraquinone. Therein, the neutralization treatment comprises treating the deposited product with sodium hydroxide in a state comprising a pH of 7-10, and subsequently treating the treated product with sodium carbonate in an amount of 0.005-0.3 pt.wt. based on the neutralization product: 1-amino-2-bromo-4- hydroxyanthraquinone.


Inventors:
FUJII TAKEO
YOKOTA TETSUYA
Application Number:
JP29008896A
Publication Date:
May 19, 1998
Filing Date:
October 31, 1996
Export Citation:
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Assignee:
SUMITOMO CHEMICAL CO
International Classes:
C07C221/00; C07C225/36; (IPC1-7): C07C225/36; C07C221/00
Attorney, Agent or Firm:
Takashi Kuboyama (1 person outside)