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Title:
PRODUCTION OF ACYLHYDROXYBENZOIC ACID
Document Type and Number:
Japanese Patent JPH10218838
Kind Code:
A
Abstract:

To produce the subject compound on an industrial scale at a low cost without using solvents by separating and purifying a crude reaction product containing the subject compound by thin-film evaporation.

The objective compound is produced by separating and purifying a reaction composition containing an acylhydroxybenzoic acid of the formula (R is a 5-17C alkyl or alkenyl; (n) is 1-3) [preferably a composition produced from a hydroxybenzoic acid (salicylic acid, p-hydroxybenzoic acid, 2,4- dihydroxybenzoic acid, 3,4,5-trihydroxybenzoic acid, etc.) using a carboxylic acid chloride or a carboxylic acid anhydride (the carboxylic acid in the structure is a 6-18C aliphatic carboxylic acid such as hexanoic acid or heptanoic acid) as an acylation agent] by thin-film evaporation preferably at an operation temperature of 140-220° under a vacuum of 0.01-1mmHg at an evaporation rate of 20-200Kg/hr.m2.


Inventors:
MORI NOBUHIRO
MIURA YASUHIRO
Application Number:
JP2531897A
Publication Date:
August 18, 1998
Filing Date:
February 07, 1997
Export Citation:
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Assignee:
LION CORP
International Classes:
B01D1/22; C07C67/08; C07C67/14; C07C67/54; C07C69/24; C07C69/28; C07C69/30; C07C69/52; (IPC1-7): C07C69/24; C07C67/08; C07C67/14; C07C67/54; C07C69/28; C07C69/30; C07C69/52
Attorney, Agent or Firm:
Hiroyuki Ikeuchi (2 outside)