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Patent Searching and Data


Title:
PRODUCTION OF ISOPHORONEDIAMINE
Document Type and Number:
Japanese Patent JPH07188126
Kind Code:
A
Abstract:

PURPOSE: To produce isophoronediamine useful as a raw material for alicyclic polyamides and coatings in high yield and purity.

CONSTITUTION: This process for the production of isophoronediamine comprises the 1st step to react isophoronpnitrile with ammonia in the presence of methanol solvent to obtain a mixture of isophoroneiminonitrile and isophoronenitrile and the 2nd step to convert the mixture into the isophoronediamine by the reducing amination with a fixed bed reactor containing a packed granular Raney cobalt maintained at 40-150°C. This process is effective for suppressing the by-production of intramolecular cyclization reaction product, completely converting an intermediate unable to be separated by distillation and getting the objective isophoronediamine in high productivity, selectivity and purity.


Inventors:
TAKAMATSU YOSHIKAZU
ADACHI TETSUTO
Application Number:
JP33633993A
Publication Date:
July 25, 1995
Filing Date:
December 28, 1993
Export Citation:
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Assignee:
ASAHI CHEMICAL IND
International Classes:
B01J25/00; C07B61/00; C07C209/48; C07C209/52; C07C211/36; (IPC1-7): C07C211/36; B01J25/00; C07C209/48; C07C209/52