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Title:
PRODUCTION OF N-LONG CHAIN ACYLIMINO DIBASIC ACID OR SALT THEREOF
Document Type and Number:
Japanese Patent JP3544454
Kind Code:
B2
Abstract:

PROBLEM TO BE SOLVED: To industrially advantageously obtain the subject compound having a good smell and stability by adding an alkaline agent into a reaction liquid containing an N-long chain acylimino dibasic acid obtained by using a specific reaction solvent and a specific production method.
SOLUTION: This method for producing an N-long chain acylimino dibasic acid or salt thereof, is provided by reacting (B) a compound of formula I [M1, M2 are each H or a cation; (m), (n) are each 1-3] with (C) an acid halide of the formula: RCOX (R is a 5-21C linear or branched alkyl, an alkenyl or the like; X is a halogen) in (A) a reaction solvent containing at least a lower alcohol, and then performing a salt exchange as necessary, or hydrolyzing (E) a compound of formula III obtained by reacting (D) a compound of formula II with the component (C) and then performing the salt exchange as necessary to obtain (F) a reaction solution containing the N-long chain acylimino dibasic acid (salt) of formula IV, then adding (G) an alkaline agent (e.g. sodium hydroxide) into the solution (F) to decompose the lower alcohol in the component (A) and an ester produced from the component (C).


Inventors:
Hidetake Nakamura
Mitsugu Morishita
Shinichiro Tanahashi
Koichi Fukuda
Application Number:
JP18514997A
Publication Date:
July 21, 2004
Filing Date:
July 10, 1997
Export Citation:
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Assignee:
Kao Corporation
International Classes:
C07C231/02; C07C231/06; C07C231/24; C07C233/47; (IPC1-7): C07C233/47; C07C231/02; C07C231/06; C07C231/24
Domestic Patent References:
JP9077728A
JP52031021A
JP54100317A
JP1045693A
JP5113717A
Attorney, Agent or Firm:
Kaoru Furuya
Takahiko Mizobe
Satoshi Furuya
Shinji Mochida