CALCIUM ALKYL PHENATE SULFIDE AND PREPARATION METHOD THEREOF, AND LUBRICATING OIL COMPRISING SAME

Title:

CALCIUM ALKYL PHENATE SULFIDE AND PREPARATION METHOD THEREOF, AND LUBRICATING OIL COMPRISING SAME

Document Type and Number:

WIPO Patent Application WO/2016/127388

Kind Code:

A1

Abstract:

A calcium alkyl phenate sulfide, prepared by a preparation method comprising the following steps: a) mixing alkyl phenol, a calcium source and base oil to obtain a mixed liquid; b) mixing the mixed liquid, ethanediol and a sulfur source to perform a sulphurization reaction to obtain a sulphurization reaction liquid; c) reacting the sulphurization reaction liquid with CO2 to perform a carbonation reaction to obtain a carbonation reaction liquid; d) extracting via a solvent and refining the carbonation reaction liquid to obtain a calcium alkyl phenate sulfide, the solvent comprising solvent oil, water and an oxygen-containing derivative of hydrocarbon. The calcium alkyl phenate sulfide prepared via the above method has a free alkyl phenol content of less than 1.5 wt%. Also provided is a lubricating oil comprising the calcium alkyl phenate sulfide.

Inventors:

FAN JINFENG (CN)
QIAO QINGWEN (CN)
WAN XINSHUI (CN)
ZHOU LIQIANG (CN)
WANG SHIPING (CN)

Application Number:

PCT/CN2015/072997

Publication Date:

August 18, 2016

Filing Date:

February 13, 2015

Export Citation:

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Assignee:

XINXIANG RICHFUL LUBE ADDITIVE CO LTD (CN)

International Classes:

C10M135/02; C10M159/22; C10N30/04

Foreign References:

CN101215248A	2008-07-09
CN101372469A	2009-02-25
CN101423483A	2009-05-06
CN102676276A	2012-09-19
US5370803A	1994-12-06
CN1145944A	1997-03-26
US3810837A	1974-05-14

Other References: