Title:
CYCLIC 1,3-DIKETONEDIIMINE COMPOUND, AND SYNTHESIS METHOD THEREFOR AND USE THEREOF
Document Type and Number:
WIPO Patent Application WO/2023/125001
Kind Code:
A1
Abstract:
A cyclic 1,3-diketonediimine compound, and a synthesis method therefor and the use thereof. The cyclic 1,3-diketonediimine compound has a structure as shown in the following general formulas I, II or III, wherein R1-R8 are each independently selected from H, halogen, and a C1-C10 saturated alkyl, where n = 0, 1 or 2. A cyclic β-diimine has a strong binding capacity to an alcohol compound; after same is combined with an alcohol compound by mean of a hydrogen bond, alcohol molecules can only be completely removed under vacuum at 95°C or higher; and the cyclic β-diimine can be used to remove trace alcohol compounds in a compound.
Inventors:
LEI JUNYU (CN)
ZHANG WEI (CN)
GAO YULI (CN)
YI JIANJUN (CN)
HONG LIUTING (CN)
HAO HAIJUN (CN)
ZHANG MINGGE (CN)
LI RONGBO (CN)
ZHANG WEI (CN)
GAO YULI (CN)
YI JIANJUN (CN)
HONG LIUTING (CN)
HAO HAIJUN (CN)
ZHANG MINGGE (CN)
LI RONGBO (CN)
Application Number:
PCT/CN2022/138917
Publication Date:
July 06, 2023
Filing Date:
December 14, 2022
Export Citation:
Assignee:
PETROCHINA CO LTD (CN)
International Classes:
C07B63/02; C07C251/20; C07C221/00; C07C225/20; C07C249/02
Foreign References:
| ES2550374A1 | 2015-11-06 | |||
| AU609125B2 | 1991-04-26 | |||
| CN104470906A | 2015-03-25 | |||
| US3622621A | 1971-11-23 | |||
| US2837568A | 1958-06-03 | |||
| DE870847C | 1953-03-16 | |||
| CN111116790A | 2020-05-08 | |||
| JP2016045391A | 2016-04-04 | |||
| US2827467A | 1958-03-18 | |||
| CN106928251A | 2017-07-07 |
Other References:
SAEED BAHJAT, MUSAD IBRAHIM: "Synthesis of Symmetrical and Non-symmetrical Diimines from Dimedone", MOLECULES, vol. 14, no. 6, 24 June 2009 (2009-06-24), pages 2278 - 2285, XP093074768, DOI: 10.3390/molecules14062278
MOSKOWITZ HENRI, ETIENNE ROUGEOT, MARCEL MIOCQUE: "Carbocyclization of acetylenic amidines", COMPTES RENDUS DES SEANCES DE L'ACADEMIE DES SCIENCES, SERIE C: SCIENCES CHIMIQUES, vol. 291, no. 13, 15 December 1980 (1980-12-15), pages 299 - 302, XP093074927
JEONG MI KIM, NA JEONG EUN, LEE CHANG GON, KIM JAE NYOUNG: "Facile Synthesis of Cyclic Vinamidinium p-Toluenesulfonates.", CHEMINFORM, ELECTROCHEMICAL SOCIETY, vol. 25, no. 2, 10 August 2004 (2004-08-10), pages 163 - 164, XP055174740, ISSN: 09317597, DOI: 10.1002/chin.200432096
MOSKOWITZ HENRI, ETIENNE ROUGEOT, MARCEL MIOCQUE: "Carbocyclization of acetylenic amidines", COMPTES RENDUS DES SEANCES DE L'ACADEMIE DES SCIENCES, SERIE C: SCIENCES CHIMIQUES, vol. 291, no. 13, 15 December 1980 (1980-12-15), pages 299 - 302, XP093074927
JEONG MI KIM, NA JEONG EUN, LEE CHANG GON, KIM JAE NYOUNG: "Facile Synthesis of Cyclic Vinamidinium p-Toluenesulfonates.", CHEMINFORM, ELECTROCHEMICAL SOCIETY, vol. 25, no. 2, 10 August 2004 (2004-08-10), pages 163 - 164, XP055174740, ISSN: 09317597, DOI: 10.1002/chin.200432096
Attorney, Agent or Firm:
BEIJING SANYOU INTELLECTUAL PROPERTY AGENCY LTD. (CN)
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