Title:
MESOPOROUS NICKEL POWDER AND PREPARATION METHOD THEREFOR, NICKEL-PHOSPHORUS CATALYST SYSTEM AND ADIPONITRILE PREPARATION METHOD
Document Type and Number:
WIPO Patent Application WO/2024/000734
Kind Code:
A1
Abstract:
A mesoporous nickel powder and a preparation method therefor, and a nickel-phosphorus catalyst system. The mesoporous nickel powder comprises powder-like particles of metallic nickel, the average particle size of the particles being 1-100 μm, the average pore diameter being 10-60 nm, the pore volume being 0.02-0.09 cm3/g, and the BET specific surface area being 5.0-40.0 m2/g. The preparation method for the mesoporous nickel powder comprises: a hydrothermal synthesis step; a templating agent removal step; and a reduction step; the templating agent is a triblock copolymer comprising an A-B-A structure, or a disulfide bond diblock copolymer comprising an A-S-S-B structure. The nickel-phosphorus catalyst system comprises a complex formed by the mesoporous nickel powder and a phosphorus ligand.
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Inventors:
CHEN ZHIRONG (CN)
WU WENBIN (CN)
LIU YAQING (CN)
MA LI (CN)
YIN HONG (CN)
HUANG GUODONG (CN)
XU YONG (CN)
ZHANG XIONGWEI (CN)
WU WENBIN (CN)
LIU YAQING (CN)
MA LI (CN)
YIN HONG (CN)
HUANG GUODONG (CN)
XU YONG (CN)
ZHANG XIONGWEI (CN)
Application Number:
PCT/CN2022/110626
Publication Date:
January 04, 2024
Filing Date:
August 05, 2022
Export Citation:
Assignee:
ZHEJIANG NHU CO LTD (CN)
UNIV ZHEJIANG (CN)
SHANDONG NHU FINE CHEMICAL SCIENCE AND TECH COMPANY LTD (CN)
UNIV ZHEJIANG (CN)
SHANDONG NHU FINE CHEMICAL SCIENCE AND TECH COMPANY LTD (CN)
International Classes:
B22F1/05; B01J31/22; B22F1/06; B22F9/22; C07C253/10; C07C255/04
Domestic Patent References:
WO2008043060A2 | 2008-04-10 |
Foreign References:
CN110743555A | 2020-02-04 | |||
CN101279256A | 2008-10-08 | |||
CN106011921A | 2016-10-12 | |||
CN113264847A | 2021-08-17 | |||
CN101069847A | 2007-11-14 |
Attorney, Agent or Firm:
LINDA LIU & PARTNERS (CN)
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