DRILLING FLUIDS

Technical Field

The present invention relates to a measurement method and assembly that enables time- dependent and non-destructive measurement of solid precipitation or sag or settlement in drilling fluids (suspension) in static conditions.

Background

Drilling fluids are used to float and remove rock cuttings or fragments, cool the drill bit, lubricate the bit and drill string, and regulate the well hydrostatic pressure in drilling applications. The well hydrostatic pressure must be maintained above the formation pressure to prevent possible fluid influx from the formation and below the formation fracture pressure to minimize formation damage. It is necessary to regulate the density of the drilling fluid by using the solids (low-density and high-density materials) suspended in the drilling fluid. It is essential to monitor the possible changes in density or to determine the change tendency in advance since the solids used in the drilling fluid formulation tend to precipitate.

Various solutions for measuring the density of drilling fluids are known in the art. Solutions utilizing acoustic, laser and nuclear magnetic resonance are examples. However, these solutions do not provide non-destructive measurement and require expensive equipment and expertizing.

In the document numbered US3782199A, a device for measuring circulating fluid or sludge density is disclosed. The assembly comprises a weight immersed in the sludge passing through a tank on the circulation line and allows monitoring of the sludge density depending on the buoyant force. Flow guiding elements are also described so that the weight is not affected by the movement of the sludge. In the document numbered US2972255A, a device for monitoring the specific gravity of fluid by means of lifting force in a tank located on the circulation line is also disclosed. Since the devices mentioned above are designed for measurements in dynamic conditions, some other phenomena like centrifugal force, as a result of assembly structure, may affect the precipitation severity and measurement accuracy. Moreover, usage of these in drilling rig systems may cause misleading results since some other incidents can cause density alteration like the entrance of formation fluids (both liquid and gas).

In the document numbered US2019316461A1, a device for measuring the depth of a well containing a liquid is disclosed. It has been disclosed that weight with a relatively smooth surface is used in the assembly.

In document numbered CN208476721U, a floating device for monitoring the density of drilling fluid flowing in mud line, using change at potentiometer value of the circuit loop, accommodated on the device, as a result of vertical movement (up and down) of the device.

Apart from the solutions mentioned above regarding the drilling fluid, some other solutions for concentration measurement are also included in the art. Document JPS5613736U discloses a system for monitoring a mixture of solid and liquid fuel in the tank. The system contains more than one weight at different depths, which allows the concentration to change due to the precipitation of the solid component and the concentration distribution according to the depth. In document JPH07103876A, a method for determining the dispersibility and precipitation tendency of a suspension containing photosensitive material, which is used to produce a fluorescent film, in which the forces exerted on a weight immersed in the suspension are measured over time is disclosed. However, the systems and methods described in these documents cannot be applied to the measurements on drilling fluids containing solid particles consisting of clays such as bentonite and some polymers together with weighting materials such as API barite.

Objects and Brief Description of the Invention

The object of the present invention is to develop a measurement method and assembly that enables the measurement of density variation of drilling fluid in static conditions due to the precipitation of the solids (weighting material) within it. The invention allows determining the time-dependent change of the density of drilling fluid and predicting its behavior non- destructively in the well. A further object of the invention is to develop a measuring assembly that allows the precipitation to be measured at temperatures representing the in-situ well conditions.

With the invention, density change measurements of drilling fluids of various densities, containing clays such as bentonite, some chemicals and polymers, and inert solid (weighting material such as API barite (BaSC )) can be carried out under static conditions.

For the objects of the invention, a measurement method has been developed that enables the time-dependent calculation of the density variation by measuring the time-dependent change of the buoyant force acting on a probe suspended in a drilling fluid containing solid particles. The measurement method of the invention also allows the calculation of the instantaneous density by instantaneously measuring the effective weight change of the probe immersed in the drilling fluid. The relationship between the change of the measured force (effective probe weight) and the precipitation of the solid particles can be modeled since the change of the measured force is the result of the change of the buoyant force due to the precipitation of the solid particles in the drilling fluid.

A measurement setup has also been developed to apply this measurement method. The said measuring assembly also comprises a heat jacket surrounding a fluid chamber that holds the drilling fluid sample at a temperature corresponding to the in-situ borehole condition.

The measuring assembly includes an ellipsoid- shaped probe whose long axis extends vertically in order to prevent the accumulation of solid particles on the probe, which causes measurement errors. The probe is made of a material with a suitable geometric shape to minimize the surface area where solid particles can adhere. A coating is applied to the surface of the probe to prevent the adhesion of solid particles. The probe is made of a high-density material, for example, lead, to sink in the drilling fluid and prevent vertical oscillation.

Detailed Description of the Invention The measuring assembly for achieving the objects of the present invention is shown in the accompanying figures.

Figure 1 It is a schematic view of a measuring apparatus according to the invention.

Figure 2 It is a graph showing the change of the effective weight measured according to the invention with respect to time.

Figure 3 It is a graph showing the time-dependent change of the fluid density calculated according to the invention.

Figure 4 It is a graph showing the change of the total amount of weighting material (API barite) precipitation calculated according to the invention with respect to time.

The parts in the figures are individually numbered, and their corresponding numbers are given below.

1. Measuring assembly

2. Probe

3. Hanger

4. Precision balance

5. Fluid chamber

6. Heat jacket

7. Heat bath

8. Pipe

9. Computer

The measurement method of the invention, basically, comprises the steps of taking the drilling fluid sample into a fluid chamber (5), suspending a probe (2), the weight of which is known and the density of which is above the maximum density that the drilling fluid can have, to the drilling fluid using a hanger (3), keeping the drilling fluid in the static state, measuring the time-dependent effective weight of the probe (2) immersed into the drilling fluid, calculating the instantaneous drilling fluid density employing the buoyancy (Archimedes’ principle) using the measured force (effective weight of probe) or the change of the drilling fluid density utilizing the change of the measured force (time-dependent effective weight of probe).

The probe (2) is suspended so that it is completely submerged in the drilling fluid and does not touch the base of the fluid chamber (5). The density of drilling fluid can be expressed in the form of the core mass (probe) or preferably the corresponding specific gravity.

Measured force, which can also be called effective weight, can be expressed as follows:

Effective weight, in this case, is expressed as follows:

In the preferred embodiment of the invention, the temperature of the sample is also regulated during the measurement so that the drilling fluid behavior can be examined under conditions similar to the wellbore or borehole.

With the measurement method of the invention, measurement at one or more depths can be taken from the drilling fluid sample.

The measurement setup (1) developed for the application of the measurement method comprises the following: a fluid chamber (5) holding the drilling fluid sample, a probe (2), the weight of which is known and the density of which is above the maximum density that the drilling fluid can have, a hanger (3) having a length that holds the probe (2) in the fluid chamber (5) so that it is completely embedded in the drilling fluid and does not contact the base of the fluid chamber (5), a precision balance (4), to which the hanger (3) is attached, allows for measurement of the net force caused by the self-weight of the probe (2) and the buoyant force generated by the drilling fluid.

The hanger (3) may be a wire or line connected to the precision balance (4) at one end or a solid arm. The hanger (3) is preferably selected such that its weight and horizontal cross- sectional area are too small with respect to the probe (2) to minimize the impact on the measurement results.

The drilling fluid sample taken into the fluid chamber (5) may be a sample prepared for trial purposes before its usage in a borehole or a sample taken from a drilling fluid circulation system.

The measuring assembly (1) of the invention also includes a heat jacket (6) that surrounds the fluid chamber (5) from the sides and ensures that the sample is kept at a specific temperature so that the drilling fluid behavior can be examined under conditions similar to the wellbore. The heat jacket (6) may be in a structure containing an annular space around the fluid chamber (5) in which a heating fluid circulates, and the desired temperature conditions are ensured therewith. This fluid can be supplied by a heat bath (7) via pipes (8) connected to the heat jacket (6).

The precision balance (4) is connected to a computer for obtaining, storing, and performing calculations of the measurement results. In addition to the precision balance (4), the heat bath (7) can also be connected to the computer to regulate the temperature. These connections can be established wired or wirelessly via an external or internal card.

The fluid chamber (5) and the heat jacket (6) may be made of transparent materials for the drilling fluid and the probe (2) to be observed visually. The fluid chamber (5) is preferably in the form of a cylinder.

The probe (2) is in the form of an ellipsoid whose vertical axis is longer than its horizontal axes. Thus, solid particles such as barite or barite along with bentonite and solid polymers accumulating on the probe (2) during measurement can be prevented, and the known mass value of probe (2) is preserved. In the invention’s preferred embodiment, the ratio of each horizontal axis length of the probe (2) to the vertical axis length is between 0.3 to 0.4. The hanger (3) is connected to the probe (2) by a cylindrical channel extending along the vertical axis of the probe (2).

A coating paint was also applied to the surface of the probe (2) in order to prevent the accumulation of solid particles on the probe (2). The ratio of the horizontal axis length of the probe (2) to the diameter of the cylindrical fluid chamber (5) is less than 0.3 so that solid particles accumulation on the probe (2) is prevented and the probe (2) does not influence the precipitation tendency of the drilling fluid.

In an exemplary embodiment of the invention, a cylindrical fluid chamber (5) with a diameter of 67 mm and an ellipsoid-shaped probe (2) with a vertical axis of 41.82 mm and horizontal axes of 13.72 mm (in a circular shape) is used. The probe (2) is positioned by means of the hanger (3) so that it is two-thirds above the depth of the drilling fluid sample from the base of the fluid chamber (5).