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Title:
METHOD FOR DETERMINING FREE RADICALS IN HIGH-TEMPERATURE OXIDE MELT
Document Type and Number:
WIPO Patent Application WO/2022/121194
Kind Code:
A1
Abstract:
A method for determining free radicals in a high-temperature oxide melt, comprising: firstly, equally dividing an oxide powder to be determined into two parts by mass, respectively placing same in two identical corundum crucibles having a polygon cross section and tamping same, placing both the corundum crucibles in a high-temperature furnace, then increasing the temperature to 1600℃ or more, and respectively maintaining the temperature for different times and then quenching; and measuring the relative average height difference of the oxide melt that has been maintained for different times at each corner of the corundum crucible, when a height difference exists, it indicates that the oxide produces free radicals during the high-temperature process, and a larger height difference indicates that the oxide melt produces more free radicals during the high-temperature process. The method can determine free radicals in a high-temperature oxide melt, and has the characteristics of a simple process and easy operation.

Inventors:
HUANG AO (CN)
LI SHENGHAO (CN)
GU HUAZHI (CN)
FU LVPING (CN)
ZHANG MEIJIE (CN)
Application Number:
PCT/CN2021/086323
Publication Date:
June 16, 2022
Filing Date:
April 11, 2021
Export Citation:
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Assignee:
UNIV WUHAN SCIENCE & TECH (CN)
International Classes:
G01N21/84; G01N25/48
Foreign References:
CN111650243A2020-09-11
CN106053503A2016-10-26
CN102495096A2012-06-13
CN105445138A2016-03-30
CN106383062A2017-02-08
CN110749719A2020-02-04
DE3416381A11985-10-10
Attorney, Agent or Firm:
BEIJING BEVON INTELLECTUAL PROPERTY AGENCY (CN)
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