Title:
METHOD FOR MANUFACTURING 1,3-PROPANEDIOL, AND MANUFACTURING DEVICE
Document Type and Number:
WIPO Patent Application WO/2014/077162
Kind Code:
A1
Abstract:
Provided are a method and device for continuously manufacturing 1,3-propanediol (1,3-PDO) by subjecting 3-hydroxypropionaldehyde (3-HPA) to a hydrogenation reaction. The ratio (L/D ratio) of the tube length and opening diameter of a fixed bed catalyst reactor for performing the hydrogenation reaction is 5 to 100, and a space velocity of 1 to 6 h-1, a temperature of 50 to 100°C, and a pressure of 10 to 17 MPa are set for the reactor to thereby inhibit the production of byproducts in the reaction process of the hydrogentation reaction. Facilities costs and operating costs can thereby be reduced.
Inventors:
KAMIKAWA MASAYUKI (JP)
MATSUO TOSHIAKI (JP)
KONDO TAKEYUKI (JP)
SASE YASUNARI (JP)
TANTO MASASHI (JP)
MATSUO TOSHIAKI (JP)
KONDO TAKEYUKI (JP)
SASE YASUNARI (JP)
TANTO MASASHI (JP)
Application Number:
PCT/JP2013/080013
Publication Date:
May 22, 2014
Filing Date:
November 06, 2013
Export Citation:
Assignee:
HITACHI LTD (JP)
International Classes:
C07C29/141; C07C31/20; B01J23/42; C07B61/00; C07C45/52; C07C45/64; C07C47/19; C07C47/22
Foreign References:
| JPH05213800A | 1993-08-24 | |||
| JP2003528066A | 2003-09-24 | |||
| JP2010013367A | 2010-01-21 | |||
| JPH0640973A | 1994-02-15 | |||
| JP2013091621A | 2013-05-16 |
Other References:
KAMIKAWA ET AL: "GLYCERINE O GENRYO TO SHITA 1,3-PROPANEDIOL GOSEI PROCESS", ABSTRACTS OF THE 44TH AUTUMN MEETING OF THE SOCIETY OF CHEMICAL ENGINEERS, vol. 44, 19 August 2012 (2012-08-19), JAPAN, pages H209
Attorney, Agent or Firm:
ISONO Michizo (JP)
Michizo Isono (JP)
Michizo Isono (JP)
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