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Title:
METHOD FOR PREPARING NARROW-DISTRIBUTION TRIETHANOLAMINE BLOCK POLYETHER, BLOCK POLYETHER, AND USE THEREOF
Document Type and Number:
WIPO Patent Application WO/2022/048099
Kind Code:
A1
Abstract:
Disclosed is a method for preparing a narrow-distribution triethanolamine block polyether, the method involving subjecting triethanolamine, as an initiator, to a polymerization reaction with ethylene oxide and epoxy propane in the presence of a certain amount of a phosphazene composite catalyst to prepare the triethanolamine block polyether. In the present application, by adding a certain amount of the phosphazene composite catalyst, the prepared triethanolamine block polyether has the characteristics of a short preparation period, a narrow distribution, a low pour point, a low foamability and a good emulsification effect. In addition, compared with traditional amine ethers, the amine ether catalyst prepared by the method has a low catalyst dosage and does not require a post-treatment refining process, such that the raw material cost and the production cost are greatly reduced, and a better technical effect is achieved.

Inventors:
SUI MEIYU (CN)
LI CHUANLIANG (CN)
LU GUOTAI (CN)
JIANG MING (CN)
QIN CHENGQUN (CN)
Application Number:
PCT/CN2021/073012
Publication Date:
March 10, 2022
Filing Date:
January 21, 2021
Export Citation:
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Assignee:
WANHUA CHEMICAL GROUP CO LTD (CN)
International Classes:
B01J31/26; C08G65/28; C08G18/48; C08G18/66
Foreign References:
CN110922580A2020-03-27
CN104448293A2015-03-25
JP2001192448A2001-07-17
JP2001270925A2001-10-02
JP2003190808A2003-07-08
US6410676B12002-06-25
Other References:
CHEN HUA, HU Z, INBAO X, ANG WANG K, ANG F, INGLIN HAO J: "Research progress on ring-opening polymerization catalyst of epoxide", HUAXUE-GONGYE-YU-GONGCHENG-JISHU = JOURNAL OF CHEMICAL INDUSTRY AND ENGINEERING, CIE / NANJING HUAGONG GONGSI JISHU ZHONGXIN, ZHONGUO SHIHUA JITUAN, NANJING,, CN, no. 2, 28 April 2008 (2008-04-28), CN , pages 40 - 45, XP055906732, ISSN: 1006-7906
ZHAO RUICHAO, YAO LI-NA;GAI DONG-JIE;GU YAO: " Research Progress on Catalysts for Synthesis of Polyether Polyol", SHANGHAI PLASTICS, SHANGHAI SOCIETY OF PLASTICS ENGINEERING TECHNOLOGY; SHANGHAI INSTITUTE OF CHEMICAL INDUSTRY, no. 1, 30 March 2016 (2016-03-30), pages 16 - 25, XP055906744, ISSN: 1009-5993, DOI: 10.16777/j.cnki.issn.1009-5993.2016.01.004
Attorney, Agent or Firm:
BEYOND ATTORNEYS AT LAW (CN)
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