METHOD FOR PREPARING PHOSPHORUS-CONTAINING LIGAND

Title:

METHOD FOR PREPARING PHOSPHORUS-CONTAINING LIGAND

Document Type and Number:

WIPO Patent Application WO/2023/206791

Kind Code:

A1

Abstract:

A method for preparing a phosphorus-containing ligand. The method comprises: mixing a phosphorus-chlorine compound, polypyridine ionic liquid porous microspheres, and an organic solvent to obtain a first preparation; mixing a compound represented by formula (2) with an organic solvent to obtain a second preparation, in formula (2), Z being a polyvalent group of aliphatic hydrocarbon or aromatic hydrocarbon containing one or more substituents, wherein the substituent is selected from a hydrogen atom, a halogen atom, C1-C10 alkyl, C1-C10 alkoxy, C1-C10 alkanoyl, aryl, heteroaryl, cyano, or nitro, and n is an integer from 1 to 8; and mixing the first preparation with the second preparation for a reaction, removing HCl generated by the reaction, filtering, and carrying out post-processing on a filtrate to obtain the phosphorus-containing ligand.

Inventors:

ZHA ZENGSHI (CN)
CHEN ZHIRONG (CN)
WU WENBIN (CN)
ZHANG TINGLAN (CN)
YIN HONG (CN)
WANG KEYAN (CN)
ZHOU LITAO (CN)
LI HAORAN (CN)
HUANG GUODONG (CN)
XU YONG (CN)

Application Number:

PCT/CN2022/102172

Publication Date:

November 02, 2023

Filing Date:

June 29, 2022

Export Citation:

Click for automatic bibliography generation Help

Assignee:

ZHEJIANG NHU CO LTD (CN)
UNIV ZHEJIANG (CN)
ZHEJIANG NHU SPECIAL MAT CO LTD (CN)
ZHEJIANG NHU NYLON MAT CO LTD (CN)

International Classes:

B01J31/02; C07F9/141; B01J31/06; B01J35/08; C07F9/145; C07F9/572; C07F9/6506; C07F9/6584

Foreign References:

CN111533767A	2020-08-14
CN114075245A	2022-02-22
CN101250200A	2008-08-27
CN102875599A	2013-01-16
CN110961055A	2020-04-07
CN101250200A	2008-08-27
CN106220681A	2016-12-14
CN102875599A	2013-01-16
CN101331144A	2008-12-24
CN100441584C	2008-12-10

Other References: