Title:
METHOD FOR PREPARING STARCH OCTENYL SUCCINATE AND APPLICATION THEREOF
Document Type and Number:
WIPO Patent Application WO/2020/093962
Kind Code:
A1
Abstract:
Provided is a method for preparing starch octenyl succinate, comprising: performing jet cooking on pre-emulsion comprising starch, alkali, water, octenyl succinic anhydride, and a low boiling solvent to obtain cooked slurry, and performing enzymatic hydrolysis to obtain the starch octenyl succinate. According to the method, reaction is performed under the condition of jet cooking and the action of high-temperature water vapor, so that intermolecular hydrogen bonds and crystal structures are rapidly destroyed; and due to a remarkable gelatinization process, starch molecular chains are sufficiently swollen, and the amorphous region of the starch is significantly increased. At the same time, the high temperature water vapor may also enable the low boiling solvent in the system to be rapidly removed; the octenyl succinic anhydride is rapidly and irregularly dispersed and separated out in the system, and is in full contact with starch granules for reaction in the high-speed liquid flow state of an ejector, so that the octenyl succinic anhydride undergoes esterification reaction at positions of the starch molecule, and a plurality of sites of the starch are remarkably substituted; and the obtained starch octenyl succinate has relatively high substitution degree and emulsification property.
Inventors:
QIU DAN (CN)
CHEN ZHIRONG (CN)
ZHU WENLI (CN)
WU KEJUN (CN)
LI JIANDONG (CN)
SHI LIFANG (CN)
QI YONG (CN)
LI QICHUAN (CN)
SHI QINGAI (CN)
CHEN ZHIRONG (CN)
ZHU WENLI (CN)
WU KEJUN (CN)
LI JIANDONG (CN)
SHI LIFANG (CN)
QI YONG (CN)
LI QICHUAN (CN)
SHI QINGAI (CN)
Application Number:
PCT/CN2019/115292
Publication Date:
May 14, 2020
Filing Date:
November 04, 2019
Export Citation:
Assignee:
ZHEJIANG NHU CO LTD (CN)
UNIV ZHEJIANG (CN)
UNIV NINGBO TECHNOLOGY (CN)
UNIV ZHEJIANG (CN)
UNIV NINGBO TECHNOLOGY (CN)
International Classes:
C08B31/04; C08B33/02; C08B35/02; C08J3/03; C08L3/06
Foreign References:
| CN102151516A | 2011-08-17 | |||
| CN103966901A | 2014-08-06 | |||
| CN104231092A | 2014-12-24 | |||
| US2661349A | 1953-12-01 | |||
| CN109517079A | 2019-03-26 |
Attorney, Agent or Firm:
HANGZHOU ZHIXIAN PATENT AGENCY (CN)
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