Title:
METHOD FOR PRODUCING (FLUOROSULFONYL)PERFLUOROALKANESULFONYLIMIDE SALT
Document Type and Number:
WIPO Patent Application WO/2016/080384
Kind Code:
A1
Abstract:
[Problem] To provide a (fluorosulfonyl)perfluoroalkanesulfonylimide salt with high selectivity with high yield.
[Solution] A (fluorosulfonyl)perfluoroalkanesulfonylimide salt is produced by: obtaining a solution containing a perfluoroalkanesulfonamide ammonium salt and ammonium halide by having ammonia react with a perfluoroalkanesulfonyl halide in a solvent (first step); separating and removing the ammonium halide contained in the solution by filtrating the thus-obtained solution (second step); obtaining a solution containing "a salt of a perfluoroalkanesulfonamide and an organic base" and ammonia by adding the organic base to the thus-obtained solution containing a perfluoroalkanesulfonamide ammonium salt (third step); and adding sulfuryl fluoride to the thus-obtained solution (fourth step).
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Inventors:
KASHIWABA TAKASHI (JP)
HARADA YUMAN (JP)
OKADA TAKUYA (JP)
SASAKI SHINTARO (JP)
NANMYO TSUTOMU (JP)
HARADA YUMAN (JP)
OKADA TAKUYA (JP)
SASAKI SHINTARO (JP)
NANMYO TSUTOMU (JP)
Application Number:
PCT/JP2015/082231
Publication Date:
May 26, 2016
Filing Date:
November 17, 2015
Export Citation:
Assignee:
CENTRAL GLASS CO LTD (JP)
International Classes:
C07C303/36; C07C311/48
Domestic Patent References:
| WO2011027867A1 | 2011-03-10 |
Foreign References:
| US5874616A | 1999-02-23 | |||
| JPH0753504A | 1995-02-28 | |||
| JPH11209338A | 1999-08-03 | |||
| JP2013241353A | 2013-12-05 | |||
| JP2011057666A | 2011-03-24 | |||
| JP2011001370A | 2011-01-06 |
Other References:
FOROPOULOS, JR. J. ET AL.: "Synthesis, Properties, and Reactions of Bis ((trifluoromethyl)sulfonyl) Imide, (CF3SO2)2NH", INORGANIC CHEMISTRY, vol. 23, no. 23, 1984, pages 3720 - 3723, XP000196672, DOI: doi:10.1021/ic00191a011
Attorney, Agent or Firm:
KOBAYASHI, Hiromichi et al. (JP)
Hiromichi Kobayashi (JP)
Hiromichi Kobayashi (JP)
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