Title:
NUCLEAR MAGNETIC RESONANCE DEVICE, AND MICROCRYSTALLINE STRUCTURE ANALYSIS METHOD
Document Type and Number:
WIPO Patent Application WO/2020/045490
Kind Code:
A1
Abstract:
The objective of the present invention is to provide a nuclear magnetic resonance device and a microcrystalline structure analysis method with which a nuclear magnetic resonance signal that is effective for crystal structure analysis can be detected, even with a specimen with which said effective nuclear magnetic resonance signal cannot conventionally be detected. A nuclear magnetic resonance device 1 which excites nuclear magnetic resonance by radiating pulsed electromagnetic waves at a sample disposed in a static magnetic field, and detects a nuclear magnetic resonance signal generated by the nuclear magnetic resonance, is provided with: a static magnetic field source 4 which generates the static magnetic field; a transmitting and receiving unit 5 for radiating the electromagnetic waves and detecting the nuclear magnetic resonance signal; a rotating mechanism 10 which causes a sample container 2 in which microcrystals 3 are suspended to rotate at a variable speed, in such a way that the sample container 2 rotates at a variable speed in the static magnetic field in order to apply a time varying magnetic field thereto to three dimensionally orientate the microcrystals; and a control unit 7 for controlling the transmitting and receiving unit 5 to radiate the electromagnetic waves in synchronism with the variable speed rotation of the sample container 2.
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Inventors:
KUSUMI RYOSUKE (JP)
TAKEDA KAZUYUKI (JP)
KIMURA TSUNEHISA (JP)
KADOMA HIROSHI (JP)
TAKEDA KAZUYUKI (JP)
KIMURA TSUNEHISA (JP)
KADOMA HIROSHI (JP)
Application Number:
PCT/JP2019/033687
Publication Date:
March 05, 2020
Filing Date:
August 28, 2019
Export Citation:
Assignee:
UNIV KYOTO (JP)
International Classes:
G01N24/00
Domestic Patent References:
| WO2013118761A1 | 2013-08-15 |
Foreign References:
| JP2008039699A | 2008-02-21 | |||
| JPH0816656B2 | 1996-02-21 | |||
| US5424644A | 1995-06-13 |
Other References:
R. KUSUMI ET AL.: "Chemical shift tensor determination using magnetically oriented microcrystal array (MOMA): 13C solid-state CP NMR without MAS", JOURNAL OF MAGNETIC RESONANCE, vol. 223, October 2012 (2012-10-01), pages 68 - 72, XP028941968, DOI: 10.1016/j.jmr.2012.08.006
OKUMURA,MANABU: "Analysis of quadrupole coupling tensor by single-crystal NMR method using the pseudo-singlecrystal sample", LECTURE ABSTRACTS OF THE 55TH ANNUAL MEETING OF THE NUCLEAR MAGNETIC RESONANCE SOCIETY OF JAPAN, P75, 2016, pages 276 - 277
KUSUMI, RYOSUKE: "Analysis of anisotropic interaction from microcrystalline powder using magnetic field orientation: From the pseudo-single-crystal to suspension of magneticfield orientation", LECTURE ABSTRACTS OF THE 57TH ANNUAL MEETING OF THE NUCLEAR MAGNETIC RESONANCE SOCIETY OF JAPAN, L1-9, 18 September 2018 (2018-09-18), pages 46 - 47
OKUMURA,MANABU: "Analysis of quadrupole coupling tensor by single-crystal NMR method using the pseudo-singlecrystal sample", LECTURE ABSTRACTS OF THE 55TH ANNUAL MEETING OF THE NUCLEAR MAGNETIC RESONANCE SOCIETY OF JAPAN, P75, 2016, pages 276 - 277
KUSUMI, RYOSUKE: "Analysis of anisotropic interaction from microcrystalline powder using magnetic field orientation: From the pseudo-single-crystal to suspension of magneticfield orientation", LECTURE ABSTRACTS OF THE 57TH ANNUAL MEETING OF THE NUCLEAR MAGNETIC RESONANCE SOCIETY OF JAPAN, L1-9, 18 September 2018 (2018-09-18), pages 46 - 47
Attorney, Agent or Firm:
SUNCREST PATENT AND TRADEMARK ATTORNEYS (JP)
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