Title:
PREPARATION METHOD FOR HIGH-CONTENT 2-METHALLYL CHLORIDE
Document Type and Number:
WIPO Patent Application WO/2019/153773
Kind Code:
A1
Abstract:
The present invention relates to a preparation method for high-content 2-methallyl chloride. the high-content 2-methallyl chloride is obtained by using a chlorination reaction solution obtained by means of the reaction of isobutene and chlorine as a raw material, and continuously rectificating the chlorination reaction solution by an isobutyl chloride separation tower, an isocrotyl chloride separation tower, and a 2-methallyl chloride separation tower, wherein an extractive rectification method is used in the separation of isocrotyl chloride. The present invention has the advantages of a small number of rectification towers required for separation, high content of obtained 2-methallyl chloride, and low energy consumption.
Inventors:
YIN HONG (CN)
CHEN ZHIRONG (CN)
WANG WEISONG (CN)
MA XIAKUN (CN)
MA ZHENXIANG (CN)
WANG YUEFEN (CN)
WAN QINGMEI (CN)
QIAN JIANFANG (CN)
DONG NAN (CN)
CHEN ZHIRONG (CN)
WANG WEISONG (CN)
MA XIAKUN (CN)
MA ZHENXIANG (CN)
WANG YUEFEN (CN)
WAN QINGMEI (CN)
QIAN JIANFANG (CN)
DONG NAN (CN)
Application Number:
PCT/CN2018/109597
Publication Date:
August 15, 2019
Filing Date:
October 10, 2018
Export Citation:
Assignee:
UNIV ZHEJIANG (CN)
ZHEJIANG HUANGMA TECH CO LTD (CN)
ZHEJIANG HUANGMA TECH CO LTD (CN)
International Classes:
C07C17/10; C07C21/067
Foreign References:
CN108164389A | 2018-06-15 | |||
CN200995994Y | 2007-12-26 | |||
CN106608811A | 2017-05-03 |
Attorney, Agent or Firm:
BEIJING ZHAOJUN UNION INTELLECTUAL PROPERTY LAW FIRM (CN)
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