Title:
PREPARATION METHOD FOR LIGHT-COLORED VITAMIN A
Document Type and Number:
WIPO Patent Application WO/2023/108327
Kind Code:
A1
Abstract:
The present application discloses a preparation method for light-colored vitamin A, comprising: reacting pentadecane phosphonate or pentadecane phosphonium salt with 2-methyl-4-acetoxy-2-butenal and alkali to generate vitamin A, wherein the content of 2-methyl-4-acetoxybutyraldehyde in the 2-methyl-4-acetoxy-2-butenal is not more than 1 wt%. The vitamin A obtained by the preparation method of the present application is light in color and high in yield, and an additional decolorization process does not need to be added.
Inventors:
LV YINGDONG (CN)
LUO ZHAOHUI (CN)
LIN LONG (CN)
ZHANG XU (CN)
CHENG XIAOBO (CN)
ZHANG TAO (CN)
ZHANG YONGZHEN (CN)
LI YUAN (CN)
LUO ZHAOHUI (CN)
LIN LONG (CN)
ZHANG XU (CN)
CHENG XIAOBO (CN)
ZHANG TAO (CN)
ZHANG YONGZHEN (CN)
LI YUAN (CN)
Application Number:
PCT/CN2021/137387
Publication Date:
June 22, 2023
Filing Date:
December 13, 2021
Export Citation:
Assignee:
WANHUA CHEMICAL GROUP CO LTD (CN)
WANHUA CHEMICAL NINGBO CO LTD (CN)
WANHUA CHEMICAL NINGBO CO LTD (CN)
International Classes:
C07C67/343; C07C69/145
Foreign References:
CN111484525A | 2020-08-04 | |||
CN111484524A | 2020-08-04 | |||
CN109651150A | 2019-04-19 | |||
US5424478A | 1995-06-13 | |||
CN113214126A | 2021-08-06 | |||
CN1097414A | 1995-01-18 | |||
CN112876395A | 2021-06-01 | |||
CN111995555A | 2020-11-27 | |||
CN105949101A | 2016-09-21 | |||
CN112457229A | 2021-03-09 | |||
CN110143874A | 2019-08-20 | |||
CN101219983A | 2008-07-16 | |||
CN103044302A | 2013-04-17 |
Other References:
ZHUANCHENG LI: " Review on Synthetic Technology of Vitamin A", CHEMICAL ENGINEERING & EQUIPMENT, vol. 2009, no. 2, 15 February 2009 (2009-02-15), pages 95 - 100, XP093071960
Attorney, Agent or Firm:
SINO-CREATIVITY INTELLECTUAL PROPERTY LAW FIRM (CN)
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