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Title:
PREPARATION METHOD FOR POLYAMINO THREE-DIMENSIONAL GRAPHENE POROUS AEROGEL, AND USE THEREOF
Document Type and Number:
WIPO Patent Application WO/2023/236699
Kind Code:
A2
Abstract:
The present invention relates to the field of water treatment, and disclosed are a preparation method for a polyamino three-dimensional graphene porous aerogel and a use thereof. The preparation method comprises: (1) dissolving a water-soluble polymerizable monomer, an initiator, and a cross-linking agent in water to obtain an aqueous phase reaction solution; (2) dispersing a hydroxyl group-containing graphene oxide and hydroxyl group-containing single layer thin wall carbon nanotubes in the aqueous phase reaction solution; (3) injecting same into a mold and performing free radical polymerization to obtain a hydrogel; (4) carrying out freeze drying to obtain a porous aerogel containing three-dimensional graphene; (5) sequentially carrying out Michael addition and condensation polymerization on a polyamine and methyl acrylate to obtain a polyamino hyperbranched polymer; and (6) utilizing the polyamino hyperbranched polymer to carry out a grafting reaction on the porous aerogel containing the three-dimensional graphene, and obtaining the polyamino three-dimensional graphene porous aerogel. The present porous aerogel may be used for complexation-adsorption treatment of heavy metal ions in wastewater, and has excellent adsorption properties.

Inventors:
JIN YANXIAN (CN)
SHEN CHUANMING (CN)
CHEN ZHANGXIN (CN)
YU BINBIN (CN)
SHEN JIAPO (CN)
YAN YEDI (CN)
JI YARU (CN)
Application Number:
PCT/CN2023/092650
Publication Date:
December 14, 2023
Filing Date:
May 08, 2023
Export Citation:
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Assignee:
JINGHUA HOLDING GROUP CO LTD (CN)
UNIV TAIZHOU (CN)
International Classes:
B01J20/26
Attorney, Agent or Firm:
ZHEJIANG GOLDEN WISOURCE INTELLECTUAL PROPERTY CO., LTD. (CN)
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