Title:
PREPARATION METHOD FOR POLYAMINO THREE-DIMENSIONAL GRAPHENE POROUS AEROGEL, AND USE THEREOF
Document Type and Number:
WIPO Patent Application WO/2023/236699
Kind Code:
A2
Abstract:
The present invention relates to the field of water treatment, and disclosed are a preparation method for a polyamino three-dimensional graphene porous aerogel and a use thereof. The preparation method comprises: (1) dissolving a water-soluble polymerizable monomer, an initiator, and a cross-linking agent in water to obtain an aqueous phase reaction solution; (2) dispersing a hydroxyl group-containing graphene oxide and hydroxyl group-containing single layer thin wall carbon nanotubes in the aqueous phase reaction solution; (3) injecting same into a mold and performing free radical polymerization to obtain a hydrogel; (4) carrying out freeze drying to obtain a porous aerogel containing three-dimensional graphene; (5) sequentially carrying out Michael addition and condensation polymerization on a polyamine and methyl acrylate to obtain a polyamino hyperbranched polymer; and (6) utilizing the polyamino hyperbranched polymer to carry out a grafting reaction on the porous aerogel containing the three-dimensional graphene, and obtaining the polyamino three-dimensional graphene porous aerogel. The present porous aerogel may be used for complexation-adsorption treatment of heavy metal ions in wastewater, and has excellent adsorption properties.
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Inventors:
JIN YANXIAN (CN)
SHEN CHUANMING (CN)
CHEN ZHANGXIN (CN)
YU BINBIN (CN)
SHEN JIAPO (CN)
YAN YEDI (CN)
JI YARU (CN)
SHEN CHUANMING (CN)
CHEN ZHANGXIN (CN)
YU BINBIN (CN)
SHEN JIAPO (CN)
YAN YEDI (CN)
JI YARU (CN)
Application Number:
PCT/CN2023/092650
Publication Date:
December 14, 2023
Filing Date:
May 08, 2023
Export Citation:
Assignee:
JINGHUA HOLDING GROUP CO LTD (CN)
UNIV TAIZHOU (CN)
UNIV TAIZHOU (CN)
International Classes:
B01J20/26
Attorney, Agent or Firm:
ZHEJIANG GOLDEN WISOURCE INTELLECTUAL PROPERTY CO., LTD. (CN)
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