Title:
REACTION CONTAINER, AND METHOD AND DEVICE FOR PRODUCING OPTICALLY ACTIVE ANTI-1,2-NITROALKANOL COMPOUND
Document Type and Number:
WIPO Patent Application WO/2015/166827
Kind Code:
A1
Abstract:
A method for producing an optically active anti-1,2-nitroalkanol compound, the method including a supplying step for continuously supplying an aldehyde compound and a C2 or higher nitroalkane compound to a reaction container, a reaction step for reacting the aldehyde compound and the C2 or higher nitroalkane compound in the reaction container and obtaining an optically active anti-1,2-nitroalkanol compound, and a discharge step for continuously discharging the optically active anti-1,2-nitroalkanol compound from the reaction container, and the reaction container including a catalyst obtained by mixing a compound represented by structural formula (1), anitroalkane compound, a neodymium-containing compound, a sodium-containing compound, and a carbon structure.
Inventors:
SHIBASAKI MASAKATSU (JP)
KUMAGAI NAOYA (JP)
HASHIMOTO KAZUKI (JP)
KUMAGAI NAOYA (JP)
HASHIMOTO KAZUKI (JP)
Application Number:
PCT/JP2015/061957
Publication Date:
November 05, 2015
Filing Date:
April 20, 2015
Export Citation:
Assignee:
MICROBIAL CHEM RES FOUND (JP)
International Classes:
C07C201/12; C07C205/32; C07B53/00; C07B61/00
Domestic Patent References:
| WO2014126008A1 | 2014-08-21 |
Other References:
TAKANORI OGAWA ET AL.: "Self-Assembling Neodymium/Sodium Heterobimetallic Asymmetric Catalyst Confined in a Carbon Nanotube Network", ANGEWANDTE CHEMIE , INTERNATIONAL EDITION, vol. 52, no. 24, 2013, pages 6196 - 6201, XP055234781, ISSN: 1433-7851
DEVARAJULU SURESHKUMAR ET AL.: "A Modified Preparation Procedure for Carbon Nanotube- Confined Nd/Na Heterobimetallic Catalyst for anti-Selective Catalytic Asymmetric Nitroaldol Reactions", JOURNAL OF ORGANIC CHEMISTRY, vol. 78, no. 22, 2013, pages 11494 - 11500, XP055234783, ISSN: 0022-3263
DEVARAJULU SURESHKUMAR ET AL.: "A Modified Preparation Procedure for Carbon Nanotube- Confined Nd/Na Heterobimetallic Catalyst for anti-Selective Catalytic Asymmetric Nitroaldol Reactions", JOURNAL OF ORGANIC CHEMISTRY, vol. 78, no. 22, 2013, pages 11494 - 11500, XP055234783, ISSN: 0022-3263
Attorney, Agent or Firm:
HIROTA, Koichi et al. (JP)
Koichi Hirota (JP)
Koichi Hirota (JP)
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