Title:
AZIDE
Document Type and Number:
Japanese Patent JP2949622
Kind Code:
B2
Abstract:
PROBLEM TO BE SOLVED: To obtain the subject compound useful for producing benzoylurea compounds capable of being used as insecticides by allowing a specific benzoyl fluoride to react with an azide compound in a solvent at a specified temperature.
SOLUTION: This benzoic acid azide of the formula: Q-CO-N3 (Q is 2,3,4,5- tetrafluorophenyl, 2,3,4-trifluoro-5-chlorophenyl or the like) is obtained by allowing a benzoyl fluoride of the formula: Q-CO-F to react with an azide compound selected from sodium azide, potassium azide, and potassium azide in a solvent (for example, chlorobenzene, dichlorobenzene, a high boiling point ether, toluene or the like) at 80 to 180°C, preferably 100 to 140°C. A reaction for producing a benzoylurea compound is carried out through a reaction of the obtained carboxylic acid azide into the isocyanate compound by a Curtius decomposition reaction.
Inventors:
BETSUHYAA HAINTSUUMANFURETSUDO
MENGERU RUDORUFU
OSUTO BARUTAA
MENGERU RUDORUFU
OSUTO BARUTAA
Application Number:
JP9217598A
Publication Date:
September 20, 1999
Filing Date:
March 23, 1998
Export Citation:
Assignee:
SHERU INTERN RISAACHI MAACHATSUPII BV
International Classes:
C07C247/24; A01N37/34; C07C67/00; C07C239/00; C07C255/57; C07C273/18; C07C275/54; C07D213/64; C07D319/20; (IPC1-7): C07C247/24; C07D213/64; C07D319/20
Other References:
【文献】米国特許4431667(US,A)
Attorney, Agent or Firm:
Kawahara Kazuho