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Title:
METHOD FOR SYNTHESIZING METAL OR ALLOY NANOPARTICLE BY SUPERCRITICAL HYDROTHERMAL REACTION UNDER REDUCTIVE ATMOSPHERE
Document Type and Number:
Japanese Patent JP2012197473
Kind Code:
A
Abstract:

To solve such a problem that metal nanoparticles are easily oxidized in a short time and unstable even the surfaces thereof are coated using various methods, and especially the coated materials are separated in water and oxidation proceeds gradually from the surface in synthesis in water under a reductive atmosphere in a conventional synthesis method of metal nanoparticles.

Metal or alloy nanoparticles, the surfaces of the generated nanoparticles being metallic, are obtained by performing a hydrothermal reduction process in subcritical or supercritical water under high temperature and high pressure conditions in the presence of an appropriate reducing agent. Thus, for example, cobalt nanoparticles of which the characteristics are excellent and the use in a wide range of areas, such as catalysts, memory materials, light-emitting materials, and optoelectronics, are anticipated can be inexpensively and stably produced by using a simple method.


Inventors:
AJIRI MASAFUMI
Application Number:
JP2011061295A
Publication Date:
October 18, 2012
Filing Date:
March 18, 2011
Export Citation:
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Assignee:
UNIV TOHOKU
International Classes:
B22F9/24; B22F9/26
Domestic Patent References:
JP3663408B22005-06-22
JP2011184725A2011-09-22
JP2011184723A2011-09-22
JP2010046625A2010-03-04
JP2005060824A2005-03-10
JP2000212611A2000-08-02
Other References:
JPN6014006627; 大原智, 樋高英嗣, ZHANG Jing, 梅津光央, 名嘉節, 阿尻雅文: 'コバルトナノ粒子の超臨界水熱合成' 粉体および粉末冶金 Vol.54 No.9, 20070915, 635-638, 社団法人 粉体粉末冶金協会
Attorney, Agent or Firm:
中野 佳直
堅田 多恵子
水野 昭宣
清水 英雄
溝渕 良一
秋庭 英樹
重信 和男
高木 祐一