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Title:
METHOD FOR SYNTHESIZING VINYLSULFONYL COMPOUND AND CURING METHOD USING THE SAME COMPOUND, AND GELATIN FILM
Document Type and Number:
Japanese Patent JP2000063346
Kind Code:
A
Abstract:

To obtain the subject compound capable of being produced in a large scale with improving workability and suppressing generation of byproducts in high yield and at a low cost by reacting a specific compound with an inorganic base.

A vinylsulfonyl compound of formula II (R1 is an alkyl; R2 to R4 are each H or a monovalent group) is obtained by reacting a compound expressed by formula I (Z1 is a group capable of being eliminated by reacting with an inorganic base and forming a vinyl group, preferably chlorine, bromine or-OSO2-CH3) with an inorganic base (preferably NaHCO3, KHCO3, Na2HPO4 or K2HPO4). For example, ethylene bis(vinylsulfonyl) acetamide is obtained by adding ethylene bis(β-sulfonylmethanesulfonylethyl)acetamide to a mixture solution of water and acetonitrile added with Na2HPO4 and reacting them. The obtained vinylsulfonyl compound is able to present a gelatin film with high quality.


Inventors:
IWAMOTO RYOHEI
KATO KATSUNORI
IKEUCHI SATORU
SUZUKI TAKAYUKI
Application Number:
JP24106498A
Publication Date:
February 29, 2000
Filing Date:
August 12, 1998
Export Citation:
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Assignee:
KONISHIROKU PHOTO IND
International Classes:
C07D251/04; C07C311/11; C07C317/08; C07C317/10; C07C317/14; C07C317/18; C07C317/24; C07C317/28; C07C317/44; C07D295/10; C08F28/02; C08L41/00; C08L89/00; C09D4/06; (IPC1-7): C07C317/08; C07C311/11; C07C317/10; C07C317/14; C07C317/18; C07C317/24; C07C317/28; C07C317/44; C07D251/04; C07D295/10; C08L41/00; C08L89/00; C09D4/06
Attorney, Agent or Firm:
Nobuaki Sakaguchi